GCMS analysis results for sample AE00843, Feb 4 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN31\00843.D Vial: 5 Acq On : 31 Jan 2002 6:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

3.50 0.08 ug/L 45160 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro­ 109 C2HC12N 003018-12-0 64 3 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 50 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 9 Abundance Scan 11 (3.499 min): 00843.D (-) m/z 74.00 100.00% 74 N

82 5000 47 Tr 38 3.50 3.60 3.70 3.80 3.90 0 .......... 10 20 ....... 30 1,40——— h50______________ 60 L 11f 1 I ’ ' ' ' i ' 1 ' * i * 70 80 l ■ । » • ■ ■ । ■ • • ■ । • 90 100 110 m/z 82.00 50.56% n/z-> Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 7l4 82

5000 A i ■ ■ ■ ‘f1 ■ । 3.50 3.60 3.70 3.80 3.90 । • > ■ > । • • • • ।

47 m/ z 76.00 25.40%

miz-> 01 ...2. AAm 10 ,

20 30 35

40 50 60 _________ L ' i ' 1 ' ' I ' 70 80 । 108 I • i • ■ ■ ■ i ■ ■ ■ > I ■ ■

90 100 110 Abundance #11644: Acetonitrile, dichloro- 714 35 i • > • • i ■ ■ ■ ■ i ■ I ' ■ ' ' I ' ' ' ' I 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 83.90 25.29% 47

■n/z-> Of 10 20 30 40 —P 50 ■ ■ i ■ ■ ■ • i ■ 60 70 Tdl 1 ‘ i ‘ 80 90 ■ i ■ ■ ' ■ i ■ 100 110 pnsy Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 7l4 3.50 3.60 3.70 3.80 3.90 rn/z 47.00 25.21%

5000 82 47 35

n/z-> 0 • i * ■ ■ ■ i 1 10 20 algallass 30 40 50 _________ L ■ i ' • ■ ■ i 1 60 70 80 in......... 90 100 110 3.50 3.60 3.70 3.80 3.90

30843.D SCAN508.M Fri Feb 01 09:19:27 2002 Page 3

NYC-WTC_000052134