GCMS analysis report for sample AE01510, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

.• Data File : C:\MSDCHEM\l\5973N\02FEB21\01510 .D Vial: 5 Acq On : 21 Feb 2002 2:17 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

3.50 0.09 ug/L 42630 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 4 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 74 Abundance Scan 11 (3.498 min): 01510.D (-) m/z 74.00 100.00% 74

82 5000 47 3.50 3.60 3.70 3.80 3.90

^tz-> 01 ...... 10 ...... 20 30 ........ 40 i.......... 50 60 1 70 80 90 I8 100 1111114 4 1 s 110 m/z 81.90 57.27% Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 47 82 5000 MM. 3.50 3.60 3.70 3.80 3.90 38 m/z 76.00 36.12% I . 95 102108 01 ■ ■ i ■ ■ ■ ■ i ■ ■ • 1 i ' ■ IiT i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ TIB । - I ' ' i ~ " ‘‘I ■ ' niz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 35 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 83.90 31.91% 47

01 1 1 I 1 1 1 1 i ‘ 1 ' ‘'l 1 1 **I*’’IS ■ 1 i ■ ■ 1 ' I ■ n*1 1 1 I 1 1 1 1 1 ' ' ' 1 I ' 1 miz-> 10 20 30 40 50 60 70 80 SO 100 110 Abundance #11642: Dichloroacetonitrite $$ Acetonitrite, dichloro- $$... ■ ■ ■ ■ i ■ ■ ‘ ■ i ■ ■ ■' i ■' ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ 74 82 3.50 3.60 3.70 3.80 3.90 m/z 47.00 25.98% 5000' 47 35

m/z-> 0- —2 10 20 30 40 — 50 60 maniji 70 T1d 80 108 • i • ■ ■ 1 i ■ ■ ‘ 1 ! ‘ 90 100 110 • 11 ....M..... 1. 3.50 3.60 3.70 3.80 3.90

01510.D HP022102.M Mon Feb 25 10:55:09 2002 Page 3

NYC-WTC_000010033