GCMS analysis results for sample AD31646, Jan 25 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02JAN22\31646.D Vial: 2 Acq On : 22 Jan 2002 1:02 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 22, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.48 0.11 ug/L 36394 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 83 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 4 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 74 Abundance Scan 9 (3.476 min): 31646.D (-) m/z 74.00 100.00% 74

82 5000 47 ■ ‘ ■ ■ i ■ ■ ■ i ■ ■ ■ ■ i1 • ‘ ■ i ■ ■ ■ ■ i ■ ■ ■ 3.50 3.60 3.70 3.80 3.90

mlz—> 1 i ' 1 1 ‘ i ■ ■ • ■ । 10 20 30 40 ‘ i ■ 50 --mmep 60 70 80 JIiB 90 ' 1 ‘ 4 • * I * ’ 100 • i ‘ ’ 110 m/z 82.00 54.18% Abundance #11643: Dichlorcacetonitrile $$ Acetonitrile, dichloro- $$... 74 47 82 5000 _A ■' ■ ■) ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ‘ ■ i' ■ ■ ■ i ■ । ■ 3.50 3.60 3.70 3.80 3.90 38 m/z 76.00 31.50% I , . 95 102108 • ■ i ‘ ■ i 1 ■ ■ ■ i ■ • i ■ ■ 14**A14*I* TBB I ■ i • ' ' 1 i 1 ‘ ' 1 i ■ ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile 74 ■ ■ ■ ■ I ■ ‘ ■ i ■ • ■ • i ■ ■ ‘ ■ i11111111 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 84.00 26.81% 47 35 ......... .. hi,,,, 18* ’ 4 1 • I , 109 ‘int 1 ■ i ' ■ ' ■ i ■ ‘ ■ i ■ 1 mfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... < • ■ ■ i • ■ ■ ‘ i ■ • ■ • j ■ • ■ * i • j । ■11 74 82 3.50 3.60 3.70 3.80 3.90 m/z 47.00 23.53% 5000 47 35

n/z-> 12 —H 10 ...1... hi.. TIB ---194 90 — 100 110 • • i ■ ■ - ■ i»■ • ■ i • ■ • • i • • • ■ i • ■ 20 30 40 50 60 70 80 3.50 3.60 3.70 3.80 3.90

31646.D SCAN508.M Thu Jan 24 13:55:34 2002 Page 3

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