DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004935–000005145

Folder label: “GCMS X 2/1/02 A 2/27/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02FEB27\02453.D Vial: 4 ‘ Acq On : 27 Feb 2002 5:47 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T.

3.49 0.10 ug/L 38295 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 74 3 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 56 4 Thietane______ 74 C3H6S 000287-27-4 9 Abundance Scan 10 (3.487 min): 02453. D (-) m/z 74.00 100.00% 74

82 5000 47 1 rI ' 1 ' 1 1 1 1 3.50 3.60 3.70 3.80 3.90 ot ' 1 1 1 ‘ ' T 1 1 ' ' I ' 1 1 1 I 1 1 1 1 I 1 1 1 1 I ’ ' 1 1 1 1 71 * ■ i 1 1 1 ' i r' 1 1 ।1 1 m/z 81.90 50.89% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 82

5000 i ■ ■ 1 1 i I ‘ ' i 1 ' 3.50 3.60 3.70 3.80 3.90 47 m/ z 83.90 30.75% . 35

m/z-> 01 1112 10 ......... 20 30 ....... 40 hi50,,.. 60 __________ L ' I ' ' ' ' I ' 70 TII 80 । 108 । ' i ■ ' 1 1 i 1 1 1 1 1 1 1 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 35 i ■ ■ ■ ■ i 1 1 1 1 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 76.00 29.00% 47 - o+ |[i ■ ■ ■ ■ i ■ ■ ■ - i ■’ "dit tn rr i i | i > | । | i | n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... "IT i ■ ■ ' ■ i' ■ ■ ■ i ■ ■ ' 'I C 74 3.50 3.60 3.70 3.80 3.90 m/z 47.00 23.06%

5000 82 47 35

n/z-> 0 .mmms- ..................... 10 ' I ' ' ' 1 I 1 20 30 I 40 50 60 70 111 80 . ............ 90 100 199 110 ■ W... MAA/) 3.50 3.60 3.70 3.80 3.90

32453.D HP022102.M Thu Feb 28 08:47:22 2002 Page 3

NYC-WTC_000005072

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NYC-WTC_000005072Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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