DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5 9 7 3N\0 2FEB2 6\02015.D Vial: 3 Acq On : 26 Feb 2002 11:57 am Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.50 0.14 ug/L 63735 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 2 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 78 3 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 4 Thietane (CAS) $$ Thiacyclobutan... 74 C3H6S 000287-27-4 43 Abundance Scan 11 (3.498 min): 02015. D (-) m/z 74.00 100.00% 74

m/z—> 5000-

Abundance Of 10 gc] 20 30 40 50 60 47

1 i ■ ■ ■ 1 i 1 70 80 i 82

■’“T1

100 #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 110 N. 3.50 3.60 3.70 3.80 3.90 m/ z 81.90 64.00%

7|4 82

5000 3.50 3.60 3.70 3.80 3.90 47 m/ z 83.90 33.59%

0! 12 35 — "lil TIPPTTTTT 108 mz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74 3.50 3.60 3.70 3.80 3.90 5000 82 m/z 76.00 32.90% 47 35 01 ... |... . .. HI,.., ...... I ‘ I ' 1 ' ' 1 1 m-1 , I ■ । । 109 ■ 1 > । i । j 1 > niz- > 10 20 30 40 50 60 70 80 90 100 110 - Abundance #11644: Acetonitrile, dichloro- 74 3.50 3.60 3.70 3.80 3.90 35 m/z 47.00 23.30%

5000 82 47

/z-> 0 1 1 । 1 1 ■ ■ i 1 1 > * । 1 10 20 30 Jill 1 ' , ' ' 40 50 ■ ■ i ' ■ ' 1 i 1 60 70 TIB 80 1 - I > * ‘ 90 100 ‘ । । ■ I । ■ 110 3.50 3.60 3.70 3.80 3.90

02015.D HP022102.M Wed Feb 27 08:34:24 2002 Page 3

NYC-WTC_000004551