GCMS analysis results, Feb 27 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB25\01136.D Vial: 3 Acq On : 25 Feb 2002 12:53 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.

3.51 0.15 ug/L 62165 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 90 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 83 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 28 Abundance Scan 12 (3.509 min): 01136. D (-) m/z 74.00 100.00% 74 82 5000 47 3.50 3.60 3.70 3.80 3.90 01 r 1pr7 111 T-J-t m/z 81.90 53.83% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 82 1 1 i1 ' 1 1 1 1 1 ■ ' i ■ 1'' 11 ‘ 111 3,50 3.60 3.70 3.80 3.90 47 m/ 2 83.90 32.22% 35

m/z-> 0 ‘d*7/*0/77In"F11 ′ 1 ' » f l < 10 20 30 40 50 60 70 80 I --19 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 35 3.50 3.60 3.70 3.80 3.90 5000 82 m/Z76.00 31.27% 47

Ol — 1‘ I ’ ■ ' 1 1 ' 1 ' i 1 ' ' 1 i 1 1 ' 1 i ■ • TIt 1 • । 1 ’ 1 1 । 1 1 ■ ■ i 1 ■ m/z-> 60 70 80 90 100 110 Abundance 10 20 30 40 50 #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 4... 74 3.50 3.60 3.70 3.80 3.90 82 m/z47.00 25.93%

5000 47

mlz-> 1 35 0 .. .......................... Ill,... ' I 1 1 ■ ‘ I ' I 10 20 30 40 50 60 70 80 । 90 100 108 110 M.... ... 3.50 3.60 3.70 3.80 3.90

01136.D HP022102.M Tue Feb 26 08:29:55 2002 Page 3 NYC-WTC_000003450