DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB01\31134.D Vial: 3 Acq On : 1 Feb 2002 4:24 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1.. .\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 3.50 0.15 ug/L 68494 1,4-Dichlorobenzene-d4 9.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 90 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 74 4 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 23 Abundance Scan 11 (3.499 min): 31134.D (-) m/z 74.00 100.00% 74

5000 82

38 47 M 3.50 3.60 3.70 3.80 3.90 ol Il..................... m/z 82.00 47.55% ' l' ■ ' 1 1 1 1 ' ' 1 1 n-1 1 ■ .................. ... . , . । . m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile 74

5000 82 11 i' 1 ■ ■ i 1' ■ ■ i ■ ■ 1 ■ i' ■1 ■ i ■1 ■ ' i

47 3.50 3.60 3.70 3.80 3.90 m/z 76.00 35.63% 35 , 109 01 ....... |.........I'..... Hl," ' I 1 1 ■ ' I ' I T.B an* I I I I II I I m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11644: Acetonitrile, dichloro- 74 35 1t.t---111111111111111111117 3.50 3.60 :3.70 3.80 3.90 5000 82 m/ Z 83.90 34.36% 47

0! 1 1 1 1 1 1 1 I 1 1 1 1 I ' 1 1 ■ I 1 T 1 ' i ' ■ ' ■ i ' TIB t ‘ । । । । । ■ 1 । । > miz- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 3.50 3.60 3.70 3.80 3.90 82 m/z 47.00 29.88%

5000 47 35

m/z-> 12 0 1 1 1 I 1 1 1 1 T1 1 1 1 1 10 20 30 — ----- 40 50 60 70 "It 80 । IIIIItIii 90 100 108 110 NAAAAA 3.50 3.60 3.70 3.80 3.90

31134.D SCAN508.M Mon Feb 04 08:41:36 2002 Page 3

NYC-WTC_000004077