GCMS blank analysis results for sample AE00275, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report • Data File : C : \MSDCHEM\1\5973N\02JAN08\00275 . D Vial: 1 Acq On : 8 Jan 2002 3:24 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 Acetonitrile, dichloro- $$ ... Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 3.48 0.12 ug/L 36441 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 72 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 53 3 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 50 4 Acetaldehyde, trichloro- (CAS) $... 146 C2HC13O 000075-87-6 35 Abundance Scan 9 (3.477 min): 00275.D (-) m/z 74.00 100.00% 7|4

5000 B4 47 ■11' ■ ■111 ■' ■ i11 •111 ■1111 ■

207 3.50 3.60 3.70 3.80 3.90 0- .................. II , |i ............ 1....... .......... I 81.90 60.83% 1 ' I .. . ......... 1 1 ' n/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 74

5000 1‘Ieuuuu—rrnur 47 34 3.50 3.60 3.70 3.80 3.90 m/ z 83.90 35.80% 35

N .....,..... 109............................................................. o1 r-p m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74 Nt 3.50 3.60 3.70 3.80 3.90 134 m/z 76.00 31.12% 5000 47 35 12 । 108...................... 01 — 1 i ' ■ ' 1 i ■ 1 ' ' । m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... -Tr-r-n-p-r i ■ ■ ■ ■ i 74 3.50 3.60 3.70 3.80 3.90 m/ Z 47.00 27.03% 47 5000 1)4

37 0 ....... jl ' ■ i ■ r ■ ■ i ' ' 1 I ■ ■ i ,192. /z-> 20 40 60 80 100 120 140 160 180 200 3.50 3.60 3.70 3.80 3.90

30275.D SCAN508.M Wed Jan 09 15:10:59 2002 Page 3

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