GCMS analysis results for sample AE00328, Jan 18 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN10\00327.D Vial: 3 * Acq On 10 Jan 2002 2:00 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 1 Dichloroacetonitrile $$ Ace... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 3.49 0.11 ug/L 35136 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 2 Dichloroacetonitrile $$ Acetonit... 109 C2HC12N 003018-12-0 83 3 Acetonitrile, dichloro- $$ Diehl... 109 C2HC12N 003018-12-0 83 4 Acetonitrile, dichloro-____________ 109 C2HC12N 003018-12-0 56 Abundance Scan 10 (3.488 min): 00327.D (-) m/z 74.00 100.00% 74

82 5000 47 38 3.50 3.60 3.70 3.80 3.90 0* VrUU" ■ H, ., Jll, ■ ■ . ■ i ■ ■ ■ • i ■I............................. m/z 81.90 50.42% m/z-> 10 20 30 40 50 60 70 80 90 1 00 110 Abundance #11643: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 74

47 82 —N. | । i । I । । k । । । i m | i r I i । i i

5000 3.50 3.60 3.70 3.80 3.90 38 m/ z 83.90 36.04% I i ■ 1 ..................... WA 1 . 95 102108 O+ ' ■ i 1 1 ■ 1 । ■ i • ' i ' 1 ■ 1 i ■ ■ ■ ■ i ■ TIit —PPTTT m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11642: Dichloroacetonitrile $$ Acetonitrile, dichloro- $$... 7l4 82 ’ ' I ’ Itr 3 50 3.60 3.70 3.80 3.90 5000 m/z 76.00 33.22% 47 35 12 I ---PP 108 0+ T 1 1 1 ' ' ' I ’ 1 ' TIit ' I ' ' 1 1 1 1 1 1 ' 1 1 ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #11641: Acetonitrile, dichloro- $$ Dichloroacetonitrile $$... 7l4 3.50 3.60 3.70 3 80 3.90 m/ z 47.00 30.04% 5000 82 47

m/z-> 0 ........................... 35 | ■ ’ i ' ' ' ■ । > 1 ■ ■ । ■ ■ ■ 11 ■ ' ■ 10 20 30 40 150............ 60 70 1 TIit 80 --109 , 90 100 110 .....MA.,AA 3.50 3.60 3.70 3.80 3.90

>0327 .D SCAN508 .M Fri Jan 11- 10:08:16 2002 Page 3

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