GCMS results for sample AE00314, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN14\00314.D Vial: 3 Acq On : 14 Jan 2002 12:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 2 Butanoic acid, 2-methyl-, m.. Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 4.63 0.13 ug/L 47666 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanoic acid, 2-methyl-, methyl... 116 C6H12O2 000868-57-5 38 2 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 38 3 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 32 4 Butanoic acid, 2-methyl-, methyl... 116 C6H1202 000868-57-5 32 Abundance Scan 110 (4.630 min): 00314.D (-) m/z 41.10 100.00% 41 57 71 88

5000 51 101 A/N I • • ■ ■ I • ’ 4.20 4.40 4.60 4.80 5.00 O’. । । . ■I...... ....... I m/ z 57.10 80.96% z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #16435: Butanoic acid, 2-methyl-, methyl ester 57 88

5000 •‘ ‘‘I" 4.20 4.40 4.60 4.80 5.00 101 m/z 71.00 80.13% 27 ....... I 33................ II | I 69 ,....... 1......... 116 । A I 0 ' i ■ ' ■ ' i ' ' ■ ■ i ■ • ’ 1 i ■ ■ 1 ' i ■ ' 1 ' i ■ 44 m/z-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #16438: Butanoic acid, 2-methyl-, methyl ester 517

41 88 i ■ ■ ■ ■ i ■ A M..A. 4.20 4.40> 4.60 4.80 5.00 5000 m/ z 88.00 77.75%

1 101 0—1 1 । । ■ ■ ■ ■ I ■ ■ ■ ’ । ■ ■ i ■ ■ T——m—n/mmm—mmT lz-> 20 30 40 50 60 70 80 90 100 110 120 Abundance #16436: Butanoic acid, 2-methyl-, methyl ester (CAS) $$ Me... 57 88 4.20 4.40 4.60 4.80 5.00 m/z 43.10 45.00% fl 5000

27 101

Tl/Z-> 0 TT 20 33 • i ■ ■ ■ ■ i 30 40 1 । 50 ■ 69 ._____ ।________ 'I.......... I 1 1 1 1 I 1 44 60 70 80 I'.... 100 90 116..110 120 A. 4AAAAA I ' ' ' • I 4.20 4.40 4.60 4.80 5.00

)0314.D SCAN508.M Tue Jan 15- 08:47:51 2002 Page 4

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