Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.
NYC-WTC_000051364–000051379Folder label: “GCMS X 1/8/02 A 1/11/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN14\00314.D Vial: 3 Acq On : 14 Jan 2002 12:09 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 14, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 2-Butenal, 3-methyl- (CAS) ... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.
4.84 0.22 ug/L 77319 1,4-Dichlorobenzene-d4 9.71
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 2-Butenal, 3-methyl- (CAS) $$ 3-... 84 C5H8O 000107-86-8 46 2 2-Butenal, 3-methyl- $$ Crotonal... 84 C5H80 000107-86-8 46 3 Furan, 2,3-dihydro-4-methyl- (CA... 84 C5H80 034314-83-5 43 4 1,3-Propanediol, 2,2-diethyl- (C. . . 132 C7H1602 000115-76-4 42 Abundance Scan 128 (4.835 min): 00314.D (-) m/z 84.00 100.00% 59 84
41 5000
50 71 207 4.40 4.60 4.80 5.00 5.20 0 i'11 ■ I TT’’ 11"111 .... I... L r1111" " 11" ' r " ' i " " i" '11 1 i " " i" " r m/z 59.10 92.64% mz-> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 Abundance #3221: 2-Butenal, 3-methyl- (CAS) $$ 3-Methyl-2-butenal $$... 84 55
5000 39 AM 27 4.40 4.60 4.80 5.00 5.20 m/z 55.10 66.83%
n/z-> 0 m— I'1'1 r''• i""i" " i'■ • ■ i‘"i ■"'i"r " • i''"i ■ ■'■ r' "i 20 30 40 50 60 70 80 90 100110120130140150160170180 190 200 210 Abundance #3222: 2-Butenal, 3-methyl- $$ Crotonaldehyde, 3-methyl- $... 84 ................ 55 4.40 460 4.80 5.00 5.20 39 m/z 41.10 51.51% 5000 27
। 69 0- ।" ■ ■ i ■ ■" i" ■ ■ i" " i1" ■ i ■ •" i " " i" r'1 ■ r " • i" " i" " i miz-> 20 30 40 50 60 70 80 90 100110 120130140150 160170180190 200210 Abundance #3351: Furan, 2,3-dihydro-4-methyl- (CAS) $$ 4-METHYL-2,3-... N M M 55 84 4.40 5.20 m/z 83.10 50.29%
5000 41
69
n/z-> 0 i" " i" " i M JU I" • • i" " I" " r ■ " r ■" r " ■ i " " i"'11" ’' i" " i •"11" ’ ■ i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 4.40 4.60 4.80 5.00 5.20
)0314 .D SCAN508.M Tue Jan 15- 08:47:51 2002 Page 5
NYC-WTC_000051372
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NYC-WTC_000051642
Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051567
Laboratory report showing GCMS analysis results for sample AE00562 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051236
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00366 conducted on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051380
Laboratory report showing GCMS analysis of sample AE00315 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052128
Laboratory report showing GCMS analysis of sample AE00843 including surrogate recovery and unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051040
Laboratory report showing GCMS analysis of sample AE00276 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052001
GCMS analysis log for sample AE00699 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051394
Laboratory report showing GCMS analysis of sample AE00321 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051206
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00328 conducted on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050334
Laboratory report for sample AD31677 documenting detection of unknown compounds and surrogate recovery on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050240
Laboratory report documenting GCMS analysis of sample AD31646 with detection of unknown compounds and surrogate recovery.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · similarity 0.998
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NYC-WTC_000051336
Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.
Filed in the same folder
NYC-WTC_000051337
Administrative label page identifying the folder range for gas chromatography-mass spectrometry records from January 8 to January 11, 2002.
Filed in the same folder
NYC-WTC_000051338
Instrument output showing total ion chromatogram and abundance data for dodecafluorotriphenylphosphine (DFTPP) calibration on January 11, 2002.
Filed in the same folder
NYC-WTC_000051340
Laboratory report listing concentrations of volatile organic compounds including nitrosamines and chlorinated solvents in sample AE00314.
Filed in the same folder
NYC-WTC_000051344
Second calibration standard report for gas chromatography-mass spectrometry analysis of sample AE00314 conducted on January 15, 2002.
Filed in the same folder