Laboratory record documenting GCMS surrogate recovery data for sample AE00279 analyzed on January 10, 2002.
NYC-WTC_000050875–000050892Folder label: “GCMS X 1/7/02 A 1/9/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\MSDCHEM\1\5973N\02JAN09\279.D Vial: 4 Acq On 9 Jan 2002 8:40 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2-Butenal, 3-methyl- $$ Cro... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T.
4.84 0.28 ug/L 130536 1,4-Dichlorobenzene-d4 9.72
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
1 2-Butenal, 3-methyl- $$ Crotonal... 84 C5H80 000107-86-8 81 2 2-Butenal, 3-methyl- (CAS) $$ 3-... 84 C5H80 000107-86-8 81 3 2-Butenal, 3-methyl- 84 C5H80 000107-86-8 72 4 Furan, 2,3-dihydro-4-methyl- (CA... 84 C5H80 034314-83-5 68 Abundance Scan 128 (4.835 min): 279. D (-) m/ z 84.05 100.00% 84
55 5000 41 59
69 4.40 4.60 4.80 5.00 5.20 4474— 38 01 ■ ■ .................. . . ■ ।. 1111 ........ I..... m/z 55.10 63.32% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3222:2-Butenal, 3-methyl- $$ Crotonaldehyde, 3-methyl- $... 8|4 55
39 AA- 5000 27 4.40 4.60 4.80 5.00 5.20 m/z 83.00 45.40% 511 44 — 69 0 ■ ■ i ■ ■ ■ ■ i' —IPPI -HH - l1" 11 " I......... rn/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3221: 2-Butenal, 3-methyl- (CAS) $$ 3-Methyl-2-butenal $$... 84 55 .............. , \A,.......... 4.40 4.60 4.80 5.00 5.20 39 m/z 41.10 43.23% 5000 27
n/z-> 44 0 T-r-p-m-J-r TPPTH ■ r1' 11' mPPPPP L 69 —PPP Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 #3224:2-Butenal, 3-methyl- 85
84 90 95
4.40 4 60 4.80 AAA 5.00 5.20 m/z 39.10 37.48%
5000 41 55
n/z-> 0 TTtETET-EE-T-rr"1‘‘"I11 *HTr 20 25 30 35 40 45 „L 50 55 .......... .. 60 65 70 ■ ■ I ' ■ ' ' I '
75 80 |.............. 85 90 95 A 4.40 A 4.60 4.80 5.00 —4 5.20
279.D SCAN508.M Thu Jan 10 11:51:49 2002 Page 6
NYC-WTC_000050885
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000050838
Quality control report for GCMS analysis of sample AE00277 showing surrogate recovery data from January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050893
Laboratory record documenting GCMS surrogate recovery data for sample AE00280 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050912
Laboratory record documenting GCMS surrogate recovery data for sample AE00281 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050948
Laboratory record documenting GCMS surrogate recovery data for sample AE00310 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051755
GCMS analysis log for sample AE00561 showing surrogate recovery and unknown compounds detected on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051549
Laboratory report showing GCMS analysis results for sample AE00556 conducted on February 1, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050977
Laboratory record documenting GCMS surrogate recovery data for sample AE00317 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050963
Laboratory record documenting GCMS surrogate recovery data for sample AE00316 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050932
Laboratory record documenting GCMS surrogate recovery data for sample AE00282 analyzed on January 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050856
Laboratory record documenting GCMS surrogate recovery data for sample AE00278 analyzed on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051531
Laboratory report showing GCMS analysis results for sample AE00555 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050813
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050814
Fragmented page from a DEP laboratory record showing method parameters and sample data fields for January 7-9, 2002 testing.
Filed in the same folder
NYC-WTC_000050817
Technical form detailing GCMS analysis results for sample AE00277 listing detected compounds and concentrations from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050821
Reference report for GCMS analysis of sample AE00277 listing compound names and qualifier values from January 9-10, 2002.
Filed in the same folder
NYC-WTC_000050825
Blank analysis report for GCMS of sample AE00277 showing compounds below method detection limits from January 10, 2002.
Filed in the same folder