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GCMS surrogate recovery results for sample AE00279, Jan 2002

Machine-extracted title · confidence 90%

Laboratory record documenting GCMS surrogate recovery data for sample AE00279 analyzed on January 10, 2002.

NYC-WTC_000050875–000050892

Folder label: “GCMS X 1/7/02 A 1/9/02

Page image
Scanned page image, NYC-WTC_000050886
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02JAN09\279.D Vial: 4 ’ Acq On : 9 Jan 2002 8:40 pm Operator: Sample : 508 scan ext 1/7 Inst : Instrumen Mise : January 9, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 4.53 ug/L 2136520 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$. .. 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 23 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 279.D (-) m/z 73.10 100.00% 73

5000 43 560 5.80 6.00 6.20 55103 1 87 n/z-> 41 0- ‘ 0′111377710 T- l’11 T1 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 ।■■■•।■ i• > i< • ‘ ■ i• >■'i'• •'I m/z __ 43.10 25.41% Abundance #36138: 3-(CYCLOHEX-3-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70

5000 560 5.80 6.00 6.20 43 m/z 45.10 9.78% 27 55 ,I 87 113 174 0 r■■’r ■"i I.... "I'""I T Hipim r.... . r " 11" " i' " ■ i i" " r n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-(1.3]dioxolan-2-ylpropyl ester 73 5.60 5 80 6.00 6.20 5000 m/z 41.10 9.29% 43 27 55 87 113 174 0 TTTMMTT M (’' ■ ■ .ii ' — I ’ ■111 ■ " ■ r ■ " i ■1" r '1 ■ i ■1" r 1" i1" ' r m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- ---4PPPPPT--+ 70 5.60 5.80 6.00 6.20 m/z 71.10 6.46% 5000

45 15 | 53 88 0 I" " I " " I । HV, PPPPT 1___ " Iri 1 T V n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

279.D SCAN508.M Thu Jan 10 11:51:50 2002 Page 7

NYC-WTC_000050886

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NYC-WTC_000050886Source: NYC Law Department, mirrored locally

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