GCMS analysis results for sample AE00247, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050539–000050557

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN24\00247.D Vial: 3 • Acq On : 24 Jan 2002 4:38 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.89 4.20 ug/L 1969800 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3’-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 28 4 Silane, tetramethyl-88 C4H12Si 000075-76-3 25 Abundance Scan 220 (5.885 min): 00247.D (-) m/ z 73.10 100.00% 73 —_

5000 43 5.60 5.80 6.00 6.20 155 it 87 103 IT Tn- I ‘ 1 ‘ ‘ 11 “ ‘ I i■“■i T‘ m/z 43.10 23.73% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180

1 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 T’T ■ I 1 ■ ‘ ■ i ■rl f i ■ ■ 5.60 5.80 6.00 6.20 43 m/z 41.10 9.22% 27 . 87 TTTTTTTT 55 H ’’100’113 ' 0—001 ‘|‘'“It 174 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 -i i fi । i 4pmn’l i ITT r i । । i । । ■ 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.22% 43 27 87 i rp m Pmprp I’55 84414’1411Tpert 113 174 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... • • * ■ । • 73 5.60 5.80 6.00 6.20 m/ z 71.10 6.57%

5000

45 15 31 , 55 I 88 1 r' ■ ■ i ■1 “ i “ Tpum—gr T-rp-TTTp-rrrp-rTTpT-rrpnT-rp-rTTp-rTT^^ ' ' I ‘ ‘ ‘ ' I ‘ ‘ 1 I ' ‘ 1 1 1 /z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

50247.D SCAN508.M Fri Jan 25 10:26:04 2002 Page 7

NYC-WTC_000050549

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NYC-WTC_000050549Source: NYC Law Department, mirrored locally

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