GCMS analysis results for sample AE03250, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03250.D Vial: 5 . Acq On : 1 Mar 2002 7:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 3-(CYCLOHEX-3'-EN-YL)PROPAN ... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 5.12 ug/L 2498900 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H1404 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 223 (5.891 min): 03250.D (-) m/z 73.10 100.00% 7)3

5000

43 5.60 5.80 6.00 6.20 ............. o1 ■ ■ । ■ i 1,155.65,1 1 ■ > 11 ■ ■ ■ ■ । n ।. । ’ ’ , 87 103■ ■ i' I ’ ’ । 'i । '" i ■' ''' i1" ■ i m/z 43.10 22.86% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

............................. 5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.16% 27 87 0 111" '' i " '1 r 4 11"55" I " ITT ,i 113 1.. 'I i ■ ■ ■ ■ i ■ ■1 • i । ■ ■ ■ ■ । 174 > j1 • ■ • i ■ ■ ■11 ■ ■' ■ >'1 ■' i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.84% 43 27 55 87 113 174 0TIIPTH 11'' ■' i " '' iI' +yr TIPWTuT m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- , m . /NP 1 1 P"1 T r1 P7 73 5.60 5.80 6.00 6.20 m/z 71.00 6.36% 5000

45 15 88 | 53 0 " i ■ Pi ■ । । ■ TO | I Pl l | lll'l'l‘| I I rrj t '11' " 11'11 ■ i ■ " 11" " i1" ' i " ‘' i " " i " " I " " I' A m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

53250.D HP022102.M Mon Mar 04 12:33:42.2002 Page 11

NYC-WTC_000006200