GCMS analysis results for sample AE03250, March 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03250.D Vial: 5 , Acq On : 1 Mar 2002 7:18 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 10 Cyclopentasiloxane, decamet... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.28 ug/L 197360 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 50 3 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 43 4 Benzoic acid, 2,4-bis[(trimethyl... 370 C16H30O4Si3 010586-16-0 37 Abundance Scan 812 (12.541 min): 03250.D (-) m/z 73.10 100.00% 73

5000 267 355

— 45 12.20 12.40 12.60 12.80 154 179 207 237 „ | 323 0+ TL .1 m/ z 266.90 48.88% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 12.20 12.40 12.60 12.80 355 m/z 355.00 48.65% 45 193 m/z-> I I 01 ■I 50 ' 1 100 i ■ 1 ' ■ 150 i ■ I

200 223.1,4.1)1 1 1 1 250 300 350 323 ■ 1 i । 1 1 1 1 400 i ' ■ 1 ■ 450 i 1

Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 12.20 12.40 12.60 12.80 267 5000 m/ z 356.00 13.13%

207 323 , | O+ ■ i ' ■1' 1 I ' 1 ' 1 1 ' 1 " i ' IT i 1 ' 1 ' i 1 1 1 ' I 1 m/z-> 50 100 150 200 250 300 350 400 450 Abundance ................................................... .. #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... 73 12.20 12.40 12.60 12.80 m/z 268.00 11.34%

5000 355

147 7 ——193 267 295 |...... 429 457 m/z-> 0 TT— 50 — — — —— 100 — 150 200 250 300 350 400 450 ....... 11 I ' 1 ' ' I ' 1 1 1 I 12.20 12.40 12.60 12.80

3250.D HP022102.M Mon Mar 04 12:33:42 2002 Page 12

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