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GCMS analysis results for sample AE01142, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01142 conducted on February 27, 2002.

NYC-WTC_000003523–000003542

Folder label: “GCMS X 1/20/02 A 2/25/02”

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Scanned page image, NYC-WTC_000003537
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01142.D Vial : 8 Acq On : 25 Feb 2002 5:01 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 9 Cyclopentasiloxane, decamet... Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T.

12.54 0.10 ug/L 62986 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 83 2 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 64 3 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H4005Si4 000000-00-0 37 4 Phenethylamine, N-methyl-.beta.,... 399 C18H37NO3Si3 010538-85-9 37 Abundance Scan 812 (12.540 min): 01142.D (-) m/ z 73.00 100.00% 73

5000 267 355 ...................................................... 45 12.20 12.40 12.60 12.80 0- IT m/z 2 67.00 47.73% m/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 .......... ............. 267 5000 12.20 12.40 12.60 12.80 m/z 355.00 40.20% 207 ........................................ ................................. O- ' ' I 1 1 I 1 1 ' T I ' ' 1 . I . . I « I I /z-> 50 100 150 200 250 300 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73 1 1 i 1 • ' * i ■ ■ 1 I ' ' ‘ ‘ I 1 ' ' ' I 12.20 12.40 12.60 12.80 5000 267 m/z 356.10 16.14% 355 45 193 n/z-> 0- 'II I' 50 ' I 1 1 1 Pri 1 11" 100 150 200 250 223.1.4 . r 300 323 11 11111 350 400 450 Abundance 73 #361636: 3,4-DIHYDROXYMANDELIC ACID-TETRATMS ■ 1 i ■ ‘ ■ 1 i ..II....... 12.20 12.40 12.60 12.80 m/ z 2 68.00 13.29% 355 5000

45 0 TI . . . . .147 193 267 295 1....... 429 457 1tT"I ′′ ‘T ‘ 1 i ■ ' ■ ' i ■ ■ rn/z-> 50 100 150 200 250 300 350 400 450 12.20 12.40 12.60 12.80

01142.D HP022102.M Tue Feb 26 08:30:35 2002 Page 11

NYC-WTC_000003537

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NYC-WTC_000003537Source: NYC Law Department, mirrored locally

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