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GCMS analysis results for sample AE03185, March 2002

Machine-extracted title · confidence 95%

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03185 conducted on March 15, 2002.

NYC-WTC_000006065–000006084

Folder label: “GCMS X 2/12/02 A 3/01/02

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Scanned page image, NYC-WTC_000006080
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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02MAR01\03185.D Vial: 5 • Acq On : 1 Mar 2002 1:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Cyclopentasiloxane, decamet... Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.33 ug/L 185496 Naphthalene-d8 13.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl - 370 C10H3005Si5 000541-02-6 64 2 (+,-)-6,7,8,14 -tetradehydro-4,5.... 355 C20H21NO5 113948-35-9 50 3 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 47 4 3,4-DIHYDROXYMANDELIC ACID-TETRATMS 472 C20H40O5Si4 000000-00-0 38 Abundance Scan 812 (12.540 min): 03185.D (-) m/z 73.00 100.00% 73

267 5000 355

45 12.20 12.40 12.60 12.80 01 - 108 133154 193 223 „ , 323- 4— m/z 266.90 54.62% n/z-> 50 100 150 200 250 300 350 400 450 Abundance #313068: Cyclopentasiloxane, decamethyl- 73

355 ........ )........ 267 5000 12.20 12.40 12.60 12.80 m/z 355.00 46.24% 207 । 323 O—T 1 1 1 1 1 1 1 1 1 1 r I PT m/z-> 50 100 150 200 250 300 350 400 450 Abundance #302413: (+,-)-6,7,8,14-tetradehydro-4,5.alpha.-epoxy-3,6-... 267 355 ........ )... . 12.20 12.40 12.60 12.80 5000 m/z 356.00 13.84%

0—TT 1 i 1 11 ’ I n/z—> 50 100 150 200 250 300 350 400 450 Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... "II "di i ■ ■ ■ ■ i 73 12.20 12.40 12.60 12.80 m/z 267.90 11.94%

5000 355

147 , . , L , , 193 , 267 295 ; 429 457 O—T T—1—T । I 1 1 » ■ I ' r ' i 1 1 ' ■ i ' ' i 1 ' 1 ' i ' ' ■ ■ i m/z—> 50 100 150 200 250 300 350 400 450 12.20 12.40 12.60 12.80

)3185.D HP022102.M Mon Mar 04 12:33:00 2002 Page 12

NYC-WTC_000006080

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NYC-WTC_000006080Source: NYC Law Department, mirrored locally

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