GCMS analysis results for sample AE03185, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03185 conducted on March 15, 2002.

NYC-WTC_000006065–000006084

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\l\5973N\02MAR01\03185.D Vial: 5 • Acq On : 1 Mar 2002 1:38 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 2-Propanone, 1,1,1-trichlor... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.00 0.38 ug/L 145663 1,4-Dichlorobenzene-d4 9.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2 -Propanone, 1,1,1-trichloro- $$. . . 160 C3H3C130 000918-00-3 83 2 2-Propanone, 1,1,1-trichloro- (C. . . 160 C3H3C130 000918-00-3 53 3 2 -Propanone, 1,1,1-trichloro- (C. . . 160 C3H3C130 000918-00-3 53 4 2-Propanone, 1,1,1-trichloro- (C. . . 160 C3H3C130 000918-00-3 53 Abundance Scan 233 (6.004 min): 03185.D (-) m/ z 43.10 100.00% 4(3

5000 — 125 63 83 97 5.60 5.80 6.20 6.40 117 0- IIIa*1*11*al 4—r 49 PPLL ■ i ■ ‘ ■ 1 ■ i i 1 1 1 ' i 1 ■ 1 ' i 1 ■ ■ 1 i ' ' m/z 124.90 14.38% Tl/Z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59081:2-Propanone, 1,1,1 -trichloro- $$ .alpha., alpha..... 43

5000 5.60 5.80 6.00 6.20 6.40 m/z 82.90 8.06% 15 0-TTIBBTTm- | 35 ......................................... 97 117 125 'I......... I TE ' ’l..........I....... 1 I 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59078: 2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43 ■ i 1 1 ■ ■ i ' ■ ■ 1 i 1 1 1 1 i 1 1 1 1 i 1 ' 5.60 5.80 6.00 6.20 6.40 5000 m/z 96.90 7.80%

01! ' | I ' ' I | I 35 ■ i ' 49 61 ■ ।'r ■ ■ i''' ■' । ■''11 D1' 82 97 117 125 ■ i ■ 'i111111 r'' ।'' । 1 1,11 ■1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59079: 2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43 5.60 5.80 6.00 6.20 6.40 m/z 47.00 7.03%

5000

97 125 0 ........... ■ ■ i ■ ■ ■ ■ I । । ' l । 35 1। ■ 9....... II 117 . Il ' ' I >>■'!■• ■ ■ । 1 ■ ' ■ । . . m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.60 5.80 6.00 6.20 6.40

)3185.D HP022102.M Mon Mar 04 12:33:00 2002 Page 11

NYC-WTC_000006079

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GCMS analysis results for sample AE03248, March 2002 · Box DEP Box 12

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