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GCMS analysis results for sample AE01140, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01140 conducted on February 27, 2002.

NYC-WTC_000003503–000003522

Folder label: “GCMS X 1/20/02 A 2/25/02

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Scanned page image, NYC-WTC_000003517
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NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02FEB25\01140.D Vial: 6 Acq On : 25 Feb 2002 3:22 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C: \DATABASE\WILEY7N. L ********************************************************************* Peak Number 9 2-Propanone, 1,1,1-trichlor... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 6.00 0.41 ug/L 158825 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 64 2 2-Propanone, 1,1,1-trichloro- $$... 160 C3H3C13O 000918-00-3 64 3 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 47 4 2-Propanone, 1,1,1-trichloro- (C... 160 C3H3C13O 000918-00-3 23 Abundance Scan 233 (6.004 min): 01140. D (-) m/ z 43.05 100.00% 43

5000

97 , I25 5.60 ' 5.80' 6.00 ' 6.20 6.40 149—12117*8, 0- > ■ i ■ • > ■ i ■ ■ ■ ■ । > 1 • । I I i । 117 . |( m/z 125.00 9.60% m/z-> 10 20 30 40 __ 50 60 70 80 90 100 110 120 130 Abundance #59078:2-Propanone, 1,1,1-trichloro- (CAS) $$ Trichloroac... 43

5000 1 i 1 1 ■ ■ । 1 ■ ■ ‘ । ' 1 ' ■ । ' 1 1 1 । 1 1 5.60 5.80 6.00 6.20 6.40 m/z 96.90 6.24% 35 49—.T । > 61l'i ■ > ■ j > । > । j82< !'■ 97 0111/r21/1/B/T—/-IT/S/IBT/C/—/T=I 117 125 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59081: 2-Propanone, 1,1,1-trichloro-$$ .alpha.,.alpha..... 43

5.60 5.80 6.00 6.20 6.40 5000 m/z 82.90 5.68% N 15 | 35 49 85 97 117 125 01 1 ■ i 1 ■ ■ ■ l'1 1 1 1 I ' ''' 1 I ' ' ‘I’i . । । । > i । j । tS ‘I’’ ‘ I . . . . I . . I I I I 1* ) > , mtz~> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #59079:2-Propanone, 1,1,1 -trichloro- (CAS) $$ Trichloroac... 43 5.60 5.80 6.00 6.20 6.40 m/z 47.00 5.53%

5000

97 125 0 1............................. 35 1 49........ -HL 11 1 । 1 1 1 i1 1 1 1 I 1 11 ' 1 11 ■1 i ‘ I/ttIt 85 117 . Il n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.60 5.80 6.00 6.20 6.40

1140.D HP022102.M Tue Feb 26 08:30:18 2002 Page 11

NYC-WTC_00000351 7

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NYC-WTC_000003517Source: NYC Law Department, mirrored locally

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