GCMS analysis results for sample AE01140, Feb 2002

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Laboratory report documenting GCMS analysis of sample AE01140 conducted on February 27, 2002.

NYC-WTC_000003503–000003522

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01140.D Vial: 6 Acq On : 25 Feb 2002 3:22 pm Operator: ‘ Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.95 0.32 ug/L 123290 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 42 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 42 3 1-Hexanol, 6-amino- 117 C6H15NO 004048-33-3 9 4 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 9 Abundance . Scan 228 (5.948 min): 01140.D (-) m/ z 73.10 100.00% 73

5000

43 ■ ' i 1 5.60' 5.80 I I 55 . 87 103 6.00 6.20 O-PTT ।.. [11 " . *h rrir . 11111,1111'11'''111111111'11111111'11 ■ i ■ ■ ■ ■ i ■ ■ ■1111' ■ i' m/z 43.10 22.07% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance j#36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

........ / ,...... 5000 5.60 5.80 6.00 6.20 43 m/z 45.00 10.80% 27 55 87 174 113 0- TT Tj-r-rr-rp-rT-q-r । 1 1 | 1 1 l1! | I I I I J I I I । | >'' 1 . | I ' । l | ‘ ‘ I I | । ‘ | ‘ ‘ | 1 ' 1 > | i1"11' Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/z 41.10 8.58% 43 27 55 , 87 113 174 0- 111 ''' 1 1 TTTT4 ‘ ।11 ■ ■ i ■' ■ * i ■ undu—n—ummpuuuuumO—mm—mttpr miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #17265:1-Hexanol, 6-amino- 30 5.60 5.80 6.00 6.20 m/z 71.00 7.60%

5000

45 56 72 87 100 ......... oV 1 ■ i ■ ■ ‘ 1 । 1 1 ■ ■ i ■ ■ 1 ‘ i ' ■ ■ 1 । 1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

01140.D HP022102.M Tue Feb 26 08:30:18 2002 Page 10

NYC-WTC_000003516

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GCMS analysis results, sample AE01139, 2,4-DDD, Feb 2002 · Box DEP Box 12

NYC-WTC_000003483

Gas chromatography-mass spectrometry analysis report for sample AE01139 detecting surrogate 2,4-DDD at 76 ug with MDL of 5.0, analyzed on 02/27/2002.

1 shared topics · Same agency, volume and box · similarity 0.998