GCMS analysis results for sample AE00844, Feb 26 2002

NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB07\00844.D Vial: 7 Acq On : 7 Feb 2002 7:24 pm Operator: . Sample : 508 scan Inst : Instrumen Mise : February 7, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T.

5.92 0.39 ug/L 152908 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 28 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 28 Abundance Scan 223 (5.920 min): 00844.D (-) m/ z 73.10 100.00%

1 73

5000 43 5.60 5.80 6.00 6.20

miz-> 0- '11 ■1'' i'' ■1 r 1 I 55 —pt m +87 103 । ■ 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 । •11 । । ■ • •. । ■ < > ■ । ■l< m/ z 43.10 25.74% Abundance #36138: 3-(CYCLOHEX-3‘-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 1 1 r i 1 1 1 1 i.............. ■ ■ ■ ’ । ′ ' ■ 1 । 5.60 5.80 6.00 6.20 43 m/z 45.10 10.05% 27 55 87 113 174 0- " I" 111111,11" rIrp’ " i " 1' , I'i IT TTTIT 11 "TTT 11 ’' ’ I n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.96% 43 27 55 , 87 113 174 0- " i " " r "'r i' TTTTTT 1" I " 1,11'1111" " I11111 ■ i " ■ ■ r '111' " ■ r ■ " i' " ' i' miz-> 10 20 30I 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... 73 ' 1 r1 1 ' 5.60 .. 5.80 6.00 , A--- 6.20 — m/z 71.10 6.36%

5000

45 15 31 | 55 88 0 .... TTTIHTTDTTTTTT 1111'11 r1" I"111' ■' ■ i ■ " ■ r 1 ‘' i ■ " 11 ■ ■ " i •11' i1 ■ < i > • ■ ■ i • ■ > ■ i • • 1 ■ i ■ ‘ > i m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

00844.D HP020702.M Thu Feb 21 09:58:16 2002 Page 6

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