GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.
NYC-WTC_000051895–000051913Folder label: “GCMS X 1/10/02 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Data File : C:\MSDCHEM\1\5973N\02JAN16\00702.D Vial: 2 . Acq On : 16 Jan 2002 3:57 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 3 -(CYCLOHEX-3’-EN-YL)PROPAN... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.89 4.46 ug/L 1637740 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual
13-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 23 4 Silane, tetramethyl- (CAS) $$ Te... 88 C4H12Si 000075-76-3 9 Abundance Scan 220 (5.885 min): 00702.D (-) m/z 73.10 100.00% 73
5000 43 TTICCnnn 1 1177 । | " 5.60 5.80 6.00 6.20
/z-> 0- ml , 87 103 *0 55 11 g*)mmmmmaUIITTRum ■ i ■ "11 ■ ■ ■11 ■ — 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 m/ z 43.10 23.69% Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73
5000- ■ 1 1 ■ i ' 5.60 6.20 43 m/ z 9.23% 27 55 87 174 0-TTTTT 1 r •1' i1' •' , i i ■ pn 113 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 T’Ir ■ 1 i ' 1 ' ■
5.60 5.80 6.00 6.20 5000 m/ z 41.10 8.87% 43 27 .. ,i 87 113 174 o1TTETUTTTT 1 r55 ■ " i " 1111 1" i"1' i ■1' ■ i ■ ■" i " " i" " i " " i I "1 ■ i" " r " 11' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4814: Silane, tetramethyl- 73 5.60 5.80 6.00 6.20 m/z 71.10 6.36%
5000
45 15 | 53 88 | 0 i'''' i ■ " ’ i' " ■ 1111 ■ i " ।' 1 " 1 ' " ' I ' ' " I " " I r" 1 1 1 1 Fr > M | ( M I | I I I I | ! I I I | | ! 1 ! | ! a Tiv । ii । । /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20
10702.D SCAN508.M Thu Jan 17 08:17:22 2002 Page 4
NYC-WTC_000051902
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NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051860
GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051948
Gas chromatography-mass spectrometry analysis of sample AE00738 conducted on 1/29/02, detecting unknown compounds and 2,4-DDD surrogate at 99 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051842
Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050519
Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052291
Laboratory report detailing GCMS scan results for sample AE00844, including detection of unknown compounds and surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051697
Laboratory report showing GCMS analysis results for sample AE00470 conducted on January 17, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000051782
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000051783
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 10 and 16, 2002.
Filed in the same folder
NYC-WTC_000051785
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051789
GCMS analysis log for sample AE00703 showing detection of nitrosamines and chlorobenzenes on January 17, 2002.
Filed in the same folder
NYC-WTC_000051794
GCMS analysis log for sample AE00703 showing blank results with compounds below detection limits on January 16, 2002.
Filed in the same folder