GCMS analysis results for sample AE00247, Jan 2002

NYC 9/11 Public Portal Document **.Z

Data File : C: \MSDCHEM\1\5973N\02JAN24\00247.D Vial: 3 • Acq On : 24' Jan 2002 4:38 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 9 Cyclopentasiloxane, decamet... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 12.54 0.06 ug/L 38254 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 45 2 M-HYDROXYPHENETHANOL 2TMS 282 C14H26O2Si2 000000-00-0 33 3 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 32 4 Benzeneacetic acid, .alpha.,3,4-... 472 C20H4005Si4 037148-65-5 25 Abundance Scan 803 (12.541 min): 00247. D (-) m/z 73.10 100.00% 73

5000 267 355

45 12.20 12.40 12.60 12.80 ‘ ‘1 ‘ ■'i 1 ' m/z 267.00 39.42% z-> 50 100 150 200 250 3(X) 350 400 450 Abundance #313065: Cyclopentasiloxane, decamethyl- 73

5000 267 ‘ I • ’ ’ ‘ f ’ ’ ‘ * I ‘ 12.20 12.40 12.60 12.80 355 m/z 355.10 36.20%

n/z-> L 45

50 —————————193 100 150 ——223 200 —— 1*I*1 250 300 323 । ‘1-*I* 350 400 450 Abundance #227925: M-HYDROXYPHENETHANOL 2TMS 73 • ■ i • • • • i > • ■ i • • ■ ■ i ■ ■ • ■ i 1 103 12.20 12.40 12.60 12.80 5000 m/z 356.10 17.80% 267

nz-> L4 50 126147 -------- 100 150 193 200 250 1 300 350 400 450 Abundance #361625: Benzeneacetic acid, .alpha.,3,4-tris[(trimethylsi... ■ ■ i ■ ■ 1 ■ i ■ ■ i • ■ • • । । • i ■ 73 12.20 12.40 12.60 12.80 m/z 74.10 10.04% 5000 355

147 i 7 193 267 295 1 429 457 ——————1—9————————— n/z—> 50 100 150 200 250 300 350 400 450 12.20 12.40 12.60 12.80

30247.D SCAN508.M Fri Jan 25 10:26:05 2002 Page 11

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