GCMS analysis results for sample AE00247, Jan 2002

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Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050539–000050557

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”

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NYC 9/11 Public Portal Document M—.Z wW*sp‘ Es w

Data File : C: \MSDCHEM\1\5973N\02JAN24\00247.D Vial: 3 Acq On : 24 Jan 2002 4:38 pm Operator: Sample : 508scan Inst : Instrumen ' Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 Pyrimidinetetramine- $$ Pyr... Concentration Rank 12 R.T. EstCono Area Relative to ISTD R.T. 16.55 0.05 ug/L 32547 Acenaphthene-dl0 18.34 Hit# Of 5 Tentative ID MW MolForm . CAS# Qual

1 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 37 2 4-HYDROXY-BICYCLO[2.2.2]OCTANONE... 140 C8H12O2 066348-59-2 23005) 3 2-Dimethylamino-4,5-dimethyl-oxa... 140 C7H12N20 000000-00-0 9 AAO 4 1,3,5,7-Tetraazatricyclo[3.3.1.1... 140 C6H12N4 000100-97-0 9 y Abundance Scan 1154 (16.549 min): 00247.D (-) m/z 140.20 100.00% 140

5000 122 172 56 71 16.20 16.40 1600 16.80 43 L •' i ■ ■1‘i■•1'I‘1 • • i‘ ■'' i I 89 THT ■ i * ■ ■' i' • ■ ■ i — "11' ■ " i1 r ■ ■ ■ ।1 m/z 172.20 28.33% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35040: Pyrimidinetetramine-$$ Pyrimidine, 2,4,5,6-tetraa... 140

5000 16.20 16.40 16.60 16.80 44 123 m/z 122.10 26.57% 71 86 96 112 | PPP I|l Hmppe nmmmmmp mz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35653:4-HYDROXY-BICYCLO[2.2.2]OCTANONE $$ Bicyclo[2.2.2]... 83 140 55 "i8 70 16.20 16.40 16.60 16.80 112 5000 97 m/z 56.10 20.78%

■ ■ i ■ ■ i ■1' ‘ i • ■ i ■ 125■ i ■ • ''' 11 ‘ " I " " I " ‘r 11 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #35431:2-Dimethylamino-4,5-dimethyl-oxazole 140 16.20 16.40 16.60 16.80 CTT m/z 136.10 18.95% 44 5000 56 111 72 125 97

T613 “ i' ■ ‘ i ■ ‘1 ■ i TIPITpT bmmmmpp ■ ■ i ■ “ 11 TIT /z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 16.20 16.40 16.60 16.80

)0247.D SCAN508.M Fri Jan 25 10:26:05 2002 Page 12

NYC-WTC_000050554

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