GCMS analysis results for sample AE00247, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050539–000050557

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document 2 upulit ASML

Data File : C:\MSDCHEM\1\5973N\02JAN24\00247.D Vial: 3 * Acq On : 24 Jan 2002 4:38 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 Phenanthrene, 9-methyl- $$ ... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.14 ug/L 104684 Phenanthrene-dl0 22.65 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 52 3 6-Methoxy-2,4-dihydroxy-1,5-naph... 192 C9H8N203 000000-00-0 50 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 49 Abundance Scan 1656 (22.280 min): 00247.D (-) m/z 192.10 100.00% 1912

5000

82 96 146 160 22.00 22.20 22.40 22.60 m/z—> 40 49 THmmmp 70 | 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 " i ■■ ■ ■ i “ flu m/z 146.10 14.73% Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 1512

.. 11... । . 1 5000 22.00 22.20 22.40 22.60 m/z 191.10 14.73% 96 165 ------- 139 152 176 111111 ■ i ■' “ i ■ ■ • ■ i ■ • • ■ i ■ ■ ■ • i ■ ■ ■ • i ■ ■' ■ i ■ ■" i ■' n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192

22.00 22.20 22.40 22.60 5000 82 m/z 193.10 14.18% 54 110

/z—> 30 a 94 160 p TTWIOppn 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 k Abundance #102277:6-Methoxy-2,4-dihydroxy-1,5-naphthyridine 1912 22.00 22.20 22.40 22.60 m/z 96.10 12.77%

5000 52 80 149 163

mmepum 108 122..1341... . 1’1—11111717 1____ 2211’3 ’ I ■ ‘ I ‘ ' 1 • I ■ ■ ’ ■ I ■ ■ ■ u •1 /z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

)0247.D SCAN508.M Fri Jan 25 10:26:05 2002 Page 13

NYC-WTC_000050555

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000050555Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

GCMS results for sample AE00697, Jan 29 2002 · Box DEP Box 28

NYC-WTC_000051860

GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.

1 shared topics · Same agency, volume and box · similarity 0.997