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GCMS analysis results for sample AE00559, Jan 2002

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Laboratory report showing GCMS analysis results for sample AE00559 conducted on January 17, 2002.

NYC-WTC_000051727–000051739

Folder label: “GCMS X 1/9/02 A 1/15/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN15\00559.D Vial: 3 Acq On : 15 Jan 2002 3:10 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 15, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Phenanthrene, 9-methyl- $$ ... Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.13 ug/L 69917 Phenanthrene-dl0 22.63

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 2 1-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 3 N-(2-methylprop-2-enyl)-2-nitrob. .. 192 C10H12N2O2 000000-00-0 50 4 fluorene-9-spiro-cyclopropane 192 C15H12 000000-00-0 45 Abundance Scan 1656 (22.280 min): 00559. D (-) m/z 192.10 100.00% 192

5000

M/S 1 / 82 96 146

m/z-> 01------------ — 160

70 80 90 100 110 120 130 140 150 160 170 -l 180 190 200 langin 22.00 22.20 22.40 22.60 m/z 191.10 15.46% Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192

5000 ' 1 I 1 1 1 1 I 1 1 ? 1 r1 1 ' 1 r1 ' 22.00 22.20 22.40 22.60 m/z 193.10 14.16%

n/z-> 0 70 80 87.. . .139.., .152 , । 165 176, T 90 100 110 120 130 140 150 160 170 180 190 200 1 i ■ 1 J Abundance #101918:1 -amino-2-methyl-4-isopropyl-thiotriazaphospholin... 159 192 pp 11 I I 1 I1 r 1 4 1 22.00 22.20 22.40 22.60 5000 m/Z 96.10 13.37%

144 177

O-T ■ l ‘ ! 1— /z-> 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 22.00 22.20 22.40 22.60 77 151 m/z 146.10 11.79% 130 144 93 104 5000 119

177 0 1 I 1 1 11 1 1 ' ' T1 I.... ...... 1 rTT . ......... A.. । , J A m/z-> 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

30559.D SCAN508.M Wed Jan 16 08:14:06 2002 Page 7

NYC-WTC_000051737

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NYC-WTC_000051737Source: NYC Law Department, mirrored locally

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