GCMS analysis results, sample AE00703, January 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AE00703 conducted on 1/28/02, detecting unknown compounds and 2,4-DDD surrogate at 117 ug with 5.0 MDL.

NYC-WTC_000051842–000051859

Folder label: “GCMS X 1/10/02 A 1/16/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00703.D Vial: 3 Acq On : 16 Jan 2002 4:47 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.15 ug/L 85641 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 72 2 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 3 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N6O 000945-24-4 53 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 49 Abundance Scan 1656 (22.280 min): 00703. D (-) m/z 192.10 100.00% 192

5000

96 146 160 • ’ i ■ ' 1 i ' 70 82 ——— 22.00 22.20 22.40 22.60 40 , 118 0 . ........................ . — ho........... . 11 ■ ■ ■ ■ l ■ ■ ■ ■ i ■ .'I'. । . 11..... m/z 191.10 16.65% n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588: 4-METHOXY-.BETA.-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 > ■ i t > 22.00 22.20 22.40 22.60 146 175 m/z 96.10 15.37% Oh 1′1—0011′011110000130 r ' ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i " ■ i • " ' i1 ■'' i' .......... I1 TT mfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 ■ • l b T ' ' 1 1 | । ' 1 > f '' ‘ 22.00 22.20 22.40 22.60 5000 m/z 193.10 14.99%

96 IRS

n/z-> 88 l 139 152 ,| 176 Of —‘I—00T0—T—1uutm—muunuuunt 30 , 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 Abundance #102009: 2,4-Diamino-6-(hydroxymethyl)pteridine $$ 6-Pteri... 163 192 22.00 22.20 22.40 22.60 m/z 146.10 14.22% A 5000

66 146 176 121 134 Oh > ■ I ■1 ‘ 11r " ‘ I ■ ‘ ' r " ' i1" 11" " i " " i' - —4— —ll ....... ll 1111 ■ -PPP mfe~> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22 40 22.60

)0703.D SCAN508.M Thu Jan 17 08:17:30 2002 Page 10

NYC-WTC_000051855

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