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← Document results/DEP Box 12/GCMS X 1/20/02 A 2/25/02
Document / 19 pages

GCMS blank analysis results, Feb 25-26 2002

Machine-extracted title · confidence 90%

Laboratory report showing GC/MS analysis results for a blank sample testing specific compounds on February 25 and 26, 2002.

NYC-WTC_000003425–000003443

Folder label: “GCMS X 1/20/02 A 2/25/02

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Scanned page image, NYC-WTC_000003441
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NYC 9/11 Public Portal Document

Data.File : C: \MSDCHEM\1\5973N\02FEB25\0116B .D Vial: 1 : Acq On : 25 Feb 2002 11:14 am Operator: Sample : lab blank 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.09 ug/L 44563 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H1203 019169-94-9 83 2 2,4-Diamino-6-(hydroxymethyl)pte... 192 C7H8N6O 000945-24-4 50 3 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 4 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2: 000000-00-0 50 Abundance Scan 1675 (22.283 min): 0116B.D (-) m/z 192.10 100.00% 1512

5000

96 T T 82 146 160 22.00 22.20 22.40 22.60

mfe-> 0 A..... —...h... 1 • ■' • । “ “ 1 ■ “ • । i“''i T 11 ■ • ‘ 1 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 4 m/z 96.00 19.99% Abundance #102588:4-METHOXY-.BETA-METHYLCINNAMIC ACID $$ 2-Butenoi... 192

108 5000 22.00 22'20 22.40 22.60 146 175 m/z 191.00 17.21% 0!1‘211‘-1‘17111111/1T70——21071270‘3 l ■" ■ i ‘ “ I" ■111 ■ *1*4411441-13 Tpaasi m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102009:2,4-Diamino-6-(hydroxymethyl)pteridine $$ 6-Pteri... 163 192

22.00 2230 22.40 22.60 5000 m/z 146.10 14.48%

66 146 176 121 134 Of ’ 1’***t****1** mm ■ । ’ 'i1. 111 । pl ’ 1+24p ’1’444 1711 _ 1141 ’1’7 mfe~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #101918:1 -amino-2-methyI-4-isopropyI-thiotriazaphospholin... 159 192 22.00 22.20 22.40 22.60 7 m/z 193.10 14.00% 5000

144 177 0 111’77711111/11101121111711"7r"$111111’"’T’’-21’11-11’113133 ■ i “ ■ ri■ ■ ■ ■ i “ i ■ ■ miz—> 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

116B.D HP022102.M Tue Feb 26 08:30:43 2002 Page 14

NYC-WTC_000003441

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NYC-WTC_000003441Source: NYC Law Department, mirrored locally

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GCMS analysis results, Feb 27 2002 · Box DEP Box 12

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Gas chromatography-mass spectrometry results for sample AE01138 identifying unknown compounds and surrogates on February 27, 2002.

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