NYC 9/11 Public Portal Document
Data.File : C:\MSDCHEM\l\5973N\02FEB25\0116B .D Vial: 1
. Acq On : 25 Feb 2002 11:14 am Operator:
Sample : lab blank 1/16 Inst : Instrumen
Mise : February 25, 2002 Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator)
Title : 508 scan method
Library : C:\DATABASE\WILEY7N.L
*********************************************************************
Peak Number 13 3,6-DIMETHYL-TRIAZOLO[4,3-B... Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
24.86 0.04 ug/L 21166 Phenanthrene-dl0 22.63
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-DIMETHYL-TRIAZOLO [4,3-B]-1,2... 149 C6H7N5 061139-71-7 5
2 3,6-Dimethyl-triazolo(4,3-b)(1,2... 149 C6H7N5 000000-00-0 5
3 (Z)-3-(2-Ethoxyethenyl)pyridine 149 C9H11NO 000000-00-0 4
4 Benzaldehyde, 4-(dimethylamino)-... 149 C9H11NO 000100-10-7 4
Abundance Scan 1903 (24.857 min): 0116B.D (-) m/z 149.00 100.00%
149
5000
41 24.60 24.80 25.00 25.20
0- aa—a ****** * '' rf m/z 149.90 9.60%
m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150
Abundance #44967:3,6-DlMETHYL-TRIAZOLO[4,3-B]-1,2,4-TRlAZINE $$ 1,2...
149
5000- 81
24.60 24.80 25.00 25.20
41 53 121
m/z 41.10 9.45%
■ i ■ ‘ ■ i ■ ■' ' i 1 ‘ ' i1 • ■ ‘ i ■ 1 1 ■ i • ■ •' I ■ ■ ■ 1 i
miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150
Abundance #44984:3,6-Dimethyl-triazolo(4,3-b)(1,2,4)-triazine
149
T T T 18T
24.60 24.80 25.00 25.20
5000 81 m/z44.00 3.92%
41 53 121
0-TTTTT 1 1 1 1111 1 ‘ I1 **1444/414.4 11 1111 l‘ 1 ■■ 11 । । । । 11 t*" ’ ’ ■ I ।
iz—> 30 40 50 60 70 80 90 100 110 120 130 140 150
Abundance #45284: (Z)-3-(2-Ethoxyethenyl)pyridine
92 121 149 24.60 24.80 25.00 25.20
83
5000
106
0-0m0pnn_ -n-p-T • i • ■ ■ • i1 • 1 1 i • ■ ■ ■ I ‘ ‘ ■ T' ‘ 1 ‘ i
nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150
0116B.D HP022102.M Tue Feb 26 08:30:43 2002 Page 15
NYC-WTC_000003442
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