GCMS blank analysis results, Feb 25-26 2002

NYC 9/11 Public Portal Document

Data.File : C:\MSDCHEM\l\5973N\02FEB25\0116B .D Vial: 1 . Acq On : 25 Feb 2002 11:14 am Operator: Sample : lab blank 1/16 Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 3,6-DIMETHYL-TRIAZOLO[4,3-B... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 24.86 0.04 ug/L 21166 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3,6-DIMETHYL-TRIAZOLO [4,3-B]-1,2... 149 C6H7N5 061139-71-7 5 2 3,6-Dimethyl-triazolo(4,3-b)(1,2... 149 C6H7N5 000000-00-0 5 3 (Z)-3-(2-Ethoxyethenyl)pyridine 149 C9H11NO 000000-00-0 4 4 Benzaldehyde, 4-(dimethylamino)-... 149 C9H11NO 000100-10-7 4 Abundance Scan 1903 (24.857 min): 0116B.D (-) m/z 149.00 100.00% 149

5000

41 24.60 24.80 25.00 25.20 0- aa—a ****** * '' rf m/z 149.90 9.60% m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #44967:3,6-DlMETHYL-TRIAZOLO[4,3-B]-1,2,4-TRlAZINE $$ 1,2... 149

5000- 81 24.60 24.80 25.00 25.20 41 53 121 m/z 41.10 9.45% ■ i ■ ‘ ■ i ■ ■' ' i 1 ‘ ' i1 • ■ ‘ i ■ 1 1 ■ i • ■ •' I ■ ■ ■ 1 i

miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #44984:3,6-Dimethyl-triazolo(4,3-b)(1,2,4)-triazine 149 T T T 18T 24.60 24.80 25.00 25.20 5000 81 m/z44.00 3.92%

41 53 121 0-TTTTT 1 1 1 1111 1 ‘ I1 **1444/414.4 11 1111 l‘ 1 ■■ 11 । । । । 11 t*" ’ ’ ■ I । iz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #45284: (Z)-3-(2-Ethoxyethenyl)pyridine 92 121 149 24.60 24.80 25.00 25.20 83

5000

106 0-0m0pnn_ -n-p-T • i • ■ ■ • i1 • 1 1 i • ■ ■ ■ I ‘ ‘ ■ T' ‘ 1 ‘ i nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150

0116B.D HP022102.M Tue Feb 26 08:30:43 2002 Page 15

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