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GCMS analysis report for sample AE01636, March 2002

Machine-extracted title · confidence 100%

GCMS laboratory results for sample AE01636 conducted on March 5, 2002, showing surrogate recovery and unknown compounds.

NYC-WTC_000010086–000010105

Folder label: “GCMS X 1/23/02 A 2/21/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report : C: \MSDCHEM\1\5973N\02FEB21\01636.D • * Data File Vial: 5 Acq On : 21 Feb 2002 6:32 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 13 3,6-DIMETHYL-TRIAZOLO[4,3-B... Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 24.86 0.04 ug/L 31105 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-DIMETHYL-TRIAZOLO[4,3-B]-1,2... 149 C6H7N5 061139-71-7 5 2 3,6-Dimethyl-triazolo (4,3-b) (1,2... 149 C6H7N5 000000-00-0 5 3 2-(2-Carboxyvinyl)pyridine, tran... 149 C8H7NO2 007340-22-9 4 4 2-(1-Methyl-2-pyrryl)imidazoline 149 C8H11N3 000000-00-0 4 Abundance Scan 1903 (24.857 min): 01636.D (-) m/z 149.00 100.00% 149

5000

iz-> O-T 30 440 50 60 70 80 90 100 110 120 130 140 150 24.60 24.80 25.00 25.20 m/z 150.00 10.60% Abundance #44967:3.6-DIMETHYL-TRlAZOLO[4,3-B]-1,2,4-TRIAZINE $$ 1,2... 149

5000 81 24.60 24.80 25.00 25.20 41 53 121 m/z 41.10 10.23%

/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #44984:3,6-Dimethyl-triazolo(4,3-b)(1,2,4)-triazine 149 ■ ■ i ■ ■ ■ ■ i ' ' I ' 1 ' 1 I ' 1 24.60 24.80 25.00 25.20 5000 81 m/z 83 .'80 6.04%

41 53 121 N i|l|l O-TT ’[ mtz—> 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #45078:2-(2-Carboxyvinyl)pyridine, trans $$ 2-Pyridineacr... 18 13 i ’ ■ ■ • i ' 104 149 24.60 24.80 25.00 25.20 m/z 49.00 0.36%

5000 A A

51 79

m/z—> 0- 1** 30 40 50 60 70 all80.... I * i. • • -1 • ■ • ■ । 90 100 110 120 130 140 150 < i < - • i "I 1 ■ ( ■ ‘ ’ I I1 24.60 24.80 25.00 25.20

01636.D HP022102.M Mon Feb 25 10:55:39 2002 Page 15

NYC-WTC_000010104

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NYC-WTC_000010104Source: NYC Law Department, mirrored locally

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

2 shared non-person entities · 1 shared topics · similarity 0.998

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