GCMS method file details for April 3-5, 2002

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Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07767.D Vial: 21 Acq On 5 Apr 2002 1:34 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1\METHODS\SCAN020403 . M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 4 3,6-Dimethyl-triazolo(4,3-b... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 33.98 0.13 ug/1 150759 Phenanthrene-dl0 30.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,6-Dimethyl-triazolo(4,3-b)(1,2... 149 C6H7N5 1000146-53-3 5 2 2-(2-Carboxyvinyl)pyridine, trans 149 C8H7NO2 007340-22-9 4 3 Oxazolidine, 3-phenyl- 149 C9H11NO 020503-92-8 4 4 Formamide, N-ethyl-N-phenyl-149 C9H11NO 005461-49-4 4 Abundance Scan 5259 (33.979 min): 07767.D (-5243) (-) m/z 149.00 100.00% 149

5000

40 33.60 33.80 34.00 34.20 34.40 01 r । । 1 । । i । 1 1 1 i । 1 i m/Z 150.00 9.47% mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66819: 3,6-Dimethyl-triazolo(4,3-b)(1,2,4)-triazine 149

5000 81 33.60 33.80 34.00 34.20 34.40 41 53 121 m/z 40.10 6.89% - Ol 1' I 1'''I'''' I 111’ I ''1 ' 1 1 . I > . I I fl n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66879: 2-(2-Carboxyvinyl)pyridine, trans 104 149

33.60 33.80 34.00 34.20 34.40 5000

51 79

m/z-> Ol ' 1 I ' ' ' ' I ' ' ' ' I ' ‘ 10 20 30 ' T1 । । 40 | । । । 50 | । 60 sipeillponsyomny) i • 1 ■ ■ ■ > i ■ ■ ■ ■ । ■ • ■ ■ ।

70 80 90 100 110 120 130 140 150 ■ 1

Abundance #66838: Oxazolidine, 3-phenyl- 91 149

77 5000

106 120 51 28 39 65

m/z-> 15 0 11 i1 ''' 1 i ■ 10 20 -l+ 58 I 4 30 40 50 60 70 80 I I I'I' I I I'I T ’111’ TITTT -I-p-T- 134 I " " I 1' I ■1 1 1 i 90 100 110 120 130 140 150

07767 .D SCAN020403.M Fri Apr 05 14:31:49 2002 Page 6

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