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GCMS analysis results for sample AE07632, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of environmental sample AE07632 conducted on April 9, 2002.

NYC-WTC_000047277–000047287

Folder label: “GCMS X 4/2/02 A 4/3/02

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Scanned page image, NYC-WTC_000047286
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020403\07631.D Vial: 21 Acq On 4 Apr 2002 3:35 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 4 Formamide, N-(2-phenylethyl)- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 39.20 0.12 ug/1 86782 Chrysene-dl2 39.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Formamide, N-(2-phenylethyl)- 149 C9H11NO 023069-99-0 3 2 Furo[2,3-c]pyridine, 2,3-dihydro... 149 C9H11NO 069022-82-8 2 3 6,7-Dimethyl-triazolo(4,3-b)(1,2... 149 C6H7N5 1000146-53-7 2 4 Benzeneethanamine, N,N-dimethyl- 145 C10H15N 001126-71-2 2 Abundance Scan 6148 (39.202 min): 07631 .D (-6144) (-) m/z 105.00 100.00% 105 149 5000 ..... . , I II, . ........ . 38.80 39.00 39.20 39.40 39.60 Oh 1’111111111101111011111111*1111-03 —-T-1I-1-0-1’-1111101011’’1—B*1’0rni m/ z 149.00 64.07% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #44742: Formamide, N-(2-phenylethyl)- 104

......................... .................... ...... 5000 30 91 58 38.80 39.00 39.20 39.40 39.60 65 . 39 51 I 78 20 ----- — oh TTTT — | 118 133 149 I 1 ■ i ■b ■ 1 I p-TT Tnr m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66928: Furo[2,3-c]pyridine, 2,3-dihydro-2,7-dimethyl- 14,9

120 5000 79 106 134 65 39 52 93 oh .... I ... — 1 I''1'I 111 I I 1 1 1 I I I < 1 I I I ' " i1111111 1.... ' 1 ' ' 1 1 * 1 1 1 1 ' I I ' ' ' 1 I /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66799: 6,7-Dimethyl-triazolo(4,3-b)(1,2,4)-triazine 149

53 68 5000 42 80

m/z-> oh 10 ■ i ■ 1 1 1 i ' 20 30 4 40 50 — 60 TI." 70 93 108 121 ,., ,i......... r....... i........... .................. ' ' I ‘Tt" । । . । I । . . > ■ । . . . . । i i r-r । i i i i‘| ! । i t । 80 90 100 110 120 130 140 150

07631.D SCAN020403.M Thu Apr 04 10:49:29 2002 Page 6

NYC-WTC_000047286

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NYC-WTC_000047286Source: NYC Law Department, mirrored locally

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