GCMS analysis results for sample AE07771, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07771.D Vial: 25 Acq On 5 Apr 2002 5:17 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C: \MSDCHEM\1\METHODS\SCAN020403 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Formamide, N-ethyl-N-phenyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

33.98 0.19 ug/1 206308 Phenanthrene-dl0 30.89 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Formamide, N-ethyl-N-phenyl- 149 C9H11NO 005461-49-4 4 2 2-(2-Carboxyvinyl)pyridine, trans 149 C8H7NO2 007340-22-9 4 3 Pyridine, pentamethyl- 149 C10H15N 003748-83-2 4 4 Oxazolidine, 3-phenyl-______________ 14 9 C9H11NO 020503-92-8 4 Abundance Scan 5259 (33.979 min): 07771 .D (-5252) (-) m/z 149.00 100.00% 1-9

5000

41 33.60 33.80 34.00 34.20 34.40 01 ) ' । । । । ' । । । । । । | । । । । । m/z 150.00 8.46% n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66902: Formamide, N-ethyl-N-phenyl- 106 149

5000 t"I"" 11 'i 1 1 r1'r 1 1 i 1 1 1 1 I ' 77 33.60 33.80 34.00 34.20 34.40 m/ Z 41.10 8.23% 93 1. .. |l... T... 121 134 01 ‘I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66879: 2-(2-Carboxyvinyl)pyridine, trans 104 1-9 ' i ' ' ■ 1 i 1 1 i 1 ' ' ' i ' 1 ' ■ i ' 33.60 33.80 34.00 34.20 34.40 5000 m/z 40.05 1.07%

51 79 0 11 ' 1 '' i ■ ■1 ■ i ■1 , , .I... _ Il.... ।111' 1'I' 1 ''i'■■ 1 i ' ' 1 'I ' । । । । । ' । । । । ■ ■ । ■ ■ ■ ■ l ■ ■ ■ ■ । । ■ t U m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #66992: Pyridine, pentamethyl- 1-9 33.60 33.80 34.00 34.20 34.40

5000

93 134

0 , , 27... 1 ,, 53 , 6i^., , 77,84 . ' I 1 1107I’i ■ 1 ' I121I'1'' 1 1 । ' ' 1 i 1 + m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150

07771.D SCAN020403.M Fri Apr 05 14:35:41 2002 Page 4

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