GCMS analysis results, sample AE07518, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07518.D Vial: 14 Acq On 4 Apr 2002 7:05 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 2 Formamide, N-(cyanomethyl)- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 3.35 0.16 ug/1 109221 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Formamide, N-(cyanomethyl)- 84 C3H4N20 005018-27-9 2 2 4-Pentenal 84 C5H80 002100-17-6 1 3 l-Penten-3-one 84 C5H80 001629-58-9 1 4 Ethyl Chloride 64 C2H5C1 000075-00-3 1 Abundance Scan 47 (3.355 min): 07518.D (-45) (-) m/z 40.10 100.00% 40

5000

49 84 3.20 3.30 3.40 3.50 3.60 3.70 3.80 Oh mmmmmmmmmmm 111" I " " I ^m/^ n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #541: Formamide, N-(cyanomethyl)- 20

84 5000

oh — 36 RululpolF861..66 ‘' I " ‘ ’ 11 ” 11"'' I' ‘ +t 40 43 I...'"I 55

■ ■ । ■1 ■ ■ ।■111 ’1 "1 3 20 3.30 3.40 3.50 3.60 3.70 3.80

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #108072: 4-Pentenal 23 41 55 11' r 1" r " 1 r " ' r 1 " i " " i " " 11' 3 20 3.30 3.40 3.50 3.60 3.70 3.80 m/z 51.00 8.92%

A/PWaoy 5000 83

n/z-> Oh ''1' Abundance „1 2.4 1-48 iil/ 461 473, m 19 26 58.. 66 69 TTH+T 14 .51 79 186 1" i11 111■" i" " i 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 #63: 1-Penten-3-one > ■ । ■ ■ ■ ■ । 11' ■ ■ i'' " i" ' ■ i ■r ■ ■ r ' 27 3.20 3.30 3.40 3.50 3.60 3.70 3.80 55 5000

84 30 3942 52 11" I " 1111 mrprr 1111111! 11 0h " I " " I " 1 T'"'11 ’ ; 11111 > 111111 ITTri 1111111 I " " . ...... n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90

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