GCMS analysis results, sample AE07518, April 2002

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Data File C:\MSDCHEM\l\DATA\020404\07518.D Vial: 14 Acq On 4 Apr 2002 7:05 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 Hydrogen azide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 3.41 0.34 ug/1 225015 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 1 2 4-(2-Acetoxyphenyl)-l-ethyl-3-me... 365 C20H19N3O4 1000222-81-6 1 3 2-Chloroethanol 80 C2H5C1O 000107-07-3 1 4 Ethanol, 2,2-dichloro- 114 C2H4C120 000598-38-9 1 Abundance Scan 56 (3.408 min): 07518.D (-52) (-) m/ z 43.10 100.00% 43

5000

320 3.40 3.60 3.80 0 TIIT i- ■ -• i""i"i•" 'I""i "i""i■ • ■ ■ i"i■ ■1'I"1 ’111"111111 r11 ■ i'1 m/z 40.10 56.67% n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #3862: Hydrogen azide 43

5000 15 320 3.40 3.60 3.80 m/z 49.10 29.70% 0-Tmmmmmmmmmmmmmmpmmmmmmpm n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #4745: 4-(2-Acetoxyphenyl)-1-ethyl-3-methyl-5-(4-nitrophen... 43 3 20 3.40 3.60 3.80 5000 m/z 51.10 3.01%

76 102 139 165 189 219 *‘*—00*nuunmmu 295 323 365 0 l‘ ‘‘I‘ISII‘IIFITAA‘S‘A‘ S‘‘‘I" n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #108328:2-Chloroethanol 31 3.20 3.40 3.60 3.80

5000

0 TI JU .. 80 T*TTTTTTTTTTTTTTTTTTTTTTTTTTTTT1*WT1TCTTITT)WTWI*TWNTTTTTTTT /z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360

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