GCMS analysis results, sample AE07515, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07515.D Vial: 11 Acq On 4 Apr 2002 4:17 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 3 Hydrogen azide Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 3.42 0.16 ug/1 112005 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hydrogen azide 43 HN3 007782-79-8 1 2 4-Amino-l-butanol 89 C4H11NO 013325-10-5 1 3 Formic acid, propyl ester 88 C4H802 000110-74-7 1 4 Ethanol, 2,2-dichloro-______________ 114 C2H4C120 000598-38-9 1 Abundance Scan 58 (3.420 min): 07515.D (-50) (-) m/ z 43.10 100.00% 43

5000 40 49 3.20 3.40 3.60 3.80 01 ‘I‘‘T p-TTTp-rTTpTnnpn-rrpnnnYrTTTjTTTT^^ m/z 40.10 34.55% PMWw\~~~--A---A m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3862: Hydrogen azide 43

5000 15 28 320 3.40 3.60 3.80

ol ' i ‘ ' r' ....... mm 11" " i' ■" ।।" i111 rrri 11 j 1111111111 >> 111111 > 11 ■ m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #783: 4-Amino-1 -butanol 33

3.20 3.40 3.60 3.80 5000

45

n/z-> 0 5 .. 1518. A 133,384111,49 10 48 53 59 70 74 89 ' i" " i ‘ "1 r " ' i "111" '1 i11" I" " 111" I" " I " 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #108322: Formic acid, propyl ester 3h

42 5000 27

39 47 0 mmgm ++ • • i •" H H 571 11" " " " 73 11 ■r ' i r ' i "'11" 88 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 i ■"11" " 11

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