GCMS analysis results, sample AE07515, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07515.D Vial: 11 Acq On 4 Apr 2002 4:17 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Acetonitrile, dichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.31 0.22 ug/1 151380 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 3 1-Propyne, 3-chloro- 74 C3H3C1 000624-65-7 5 4 1-Propyne, 3-chloro-_______________ 74 C3H3C1 000624-65-7 5 Abundance Scan 40 (3.314 min): 07515. D (-36) (-) m/z 74.00 100.00% 74

5000 82

48 t ■... i. । i ■ ■ > • i ■ > ■ ‘ i ■ ■ ■ ■ । 3.20 3.30 3.40 3.50 3.60 3.70 0 ■ ■ i ■ ■ ■ . i . ■ . . j ■' 1 TIl i ' ■ ' ' i 1 1 1 1 1 1 TT i ■ । > ■ ■ ■ । ■ i > > । ■ 1 । m/z 82.00 48.92% 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 r ' " i' ■. • r ■' ■ r " 11

47 3.20 3.30 3.40 3.50 3.60 3.70 m/ Z 76.00 33.53% 35

Tl/Z-> 12 01 Trrr , ।-|—r 10 20 214— 30 40 50 62.......i .1 ■ ■ i ‘ 60 70 80 TI1 , 108 1 ■ i < ■ • • I 1 1 1 i■I ■ । 1 1 I

90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 ■' i ■ ■ 3.20 3.30 3.40 3.50 3.60 3.70 5000 82 m/z 84.00 33.28%

0! > . l . > ■ ■ I ■ < . . । 47

. i — ■ ' i ' ■ ■ ■ i ' 1 ' i ■ ' ■ ' I 1 1 1 1 I 1 ' 1 1 I /MMyut n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #108401:1-Propyne, 3-chloro- '' i1' . ......... ।।।। 39 3.20 3.30 3.40 3.50 3.60 3.70 m/ Z 48.10 25.99% 5000 74

Tl/Z-> 0 ....... 10 ,26.30 .'I 44 20 40 7.57 50 ......70 'Mm80.. 90 60 ■ ■ । ■ i 11 1 1 i 1 1 '11 100 110 111 n ' 11 " i1' " i " ■ ■ i " ■ .............. .. 3.20 3.30 3.40 3.50 3.60 3.70

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