GCMS surrogate recovery data for sample AE04945, April 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020410\04945.D Vial: 11 Acq On : 10 Apr 2002 7:47 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1... \SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************** Peak Number 1 Acetonitrile, dichloro- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 3.32 0.43 ug/1 288088 1,4-Dichlorobenzene-d4 10.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 50 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 50 3 1-Propyne, 3-chloro- 74 C3H3C1 000624-65-7 4 4 1-Propyne, 3-chloro- 74 C3H3C1 000624-65-7 3 Abundance Scan 40 (3,314 min): 04945. D (-28) (-) m/ z 74.00 100.00% 74

82 5000 40 47 ........ ...... ............ ■ ■ i ■ • ■1 I ■1 ■ ■ i • ■ ■ ■ I'1 >11 > 11 ■ I ■ ■ > ■ I 3.20 3.30 3.40 3.50 3.60 3.70 — m/z82.00 O+ i ‘ 1 ■ 1 i 1 ■ ■ ■ i ■ ' 1 i 1 1 1 1 i 1 1 1 1 i 52.69% m/z- > 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 " i''1'1'' " i " " I " 111 " 11111111 3.20 3.30 3.40 3.50 3.60 3.70 47 m/z84.00 33.61%

Ot T I I I I I I I l t I I j l 11 I ' 1 th ' ' ' 1 । ■ 1 ■ ■ । ■ 193 1 1 i ■ ‘ 1 ' i 1 1 1 1 i ' 1 ' 1 i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74 11111111111111711110 —E1ITITTT 3.20 3.30 3.40 3.50 3.60 3.70 5000 82 m/z 76.00 29.58% 47 35

m/z-> Of 12 ■ ■ l 1 • > > I ■ 10 201 2 h.... . 30 40 50 60 70 80 TI3 , 90 100 108 110 Abundance #108401: 1 -Propyne, 3-chloro- ■ ■ i11

Am " i'1" i " " i ■ ■ ■' i " " i 39 3.20 3,30 3.40 3.50 3.60 3.70 m/z 47.00 26.53%

5000 74

0 ..................... .. 47 57 -------- I 1 'T' 1 1 r I 1 1 i11' ■ i ■' ■' i " " I " 11111111r’1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.30 3.40 3.50 3.60 3.70

04945.D SCANAPR0902.M Thu-Apr 11 14:06:51 2002 Page 3

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