GCMS analysis results, sample AE07516, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07516.D Vial: 12 Acq On 4 Apr 2002 5:13 pm Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Acetonitrile, dichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

3.32 0.30 ug/1 223965 1,4-Dichlorobenzene-d4 10.66 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 39 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 38 3 Ethanol, 2-methoxy- 76 C3H802 000109-86-4 4 4 l-Propyne, 3-chloro- 74 C3H3C1 000624-65-7 4 Abundance Scan 41 (3.320 min): 07516.D (-37) (-) m/z 74.00 100.00% 74 82 5000 47

-mm 3.20 3.30 3.40 3.50 3.60 3.70 0 i ■ ' ■ ■ i ■ ■ ' ' i ■ 7k , | > i i-|-|-r-r r i' | i i ! I | m/z 82.00 56.50% n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 82 TITT TT11‘111711"1t111"131 47 3.20 3.30 3.40 3.50 3.60 3.70 m/ z 47.00 44.21% 35 Of , , ....... . , , 1 , , III , i । | । ’ । । | r I I > | । ■ I I | > ■ > i | ■ 62....... 1 1 ' I 1 1 1 1 I’1 TIil , 108 ' ' i 1 1 ' ' i 1 ' 1 1 I ' 1 ■ ■ i n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 11" 11111111 3.20 3.30 3.40 3.50 3.60 3.70 5000 82 m/z 84.00 31.48%

n/z-> 0

Abundance ■ i ■ ' ■ 1 i ■ ■ ■ ■ i ■ 10 20 30 40 47

I 1 I’i 1 1 ■ ■ i 1 ■ ' ' I ' 50 60 #110760: Ethanol, 2-methoxy- 70 TT 80 1 ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । 90 100 110 । । A 1 " " i ■ " ■ I ‘" i1 ‘1' i ’111111111 45 3.20 3.30 3.40 3.50 3.60 3.70 m/z 76.00 27.36% 5000 I 31

m/z-> 0 ....... 10 20 MLn.. 30 40 ’. L 50 60 70 80 90 100 110 1 ■ i ' ‘ ' 1 i ■ 1 1 1 i 1 ■ 1 ' i ' ' ' ' i ■ ■ ' ' i 1 1 r ' i 1 1 1 ■ i ■ ■ i'1 1' i " " i ■11111111111111 3.20 3.30 3.40 3.50 3.60 3.70

NYC-WTC_000047396