GCMS analysis results for sample AE07768, April 18, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020404\07768.D Vial: 22 Acq On 5 Apr 2002 2:30 am Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020403.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 2 Acetonitrile, dichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

3.32 0.21 ug/1 129593 1,4-Dichlorobenzene-d4 10.66

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 40 3 Thiirane, methyl- 74 C3H6S 001072-43-1 4 4 Propanoic acid 74 C3H602 000079-09-4 2 Abundance Scan 40 (3.314 min): 07768.D (-37) (-) m/z 74.00 100.00% 7|4

5000 82 40 47 ‘ I’’ • ■ i - ■ • ■ i ■ "17171 11111111 3.20 3.30 3.40 3.50 3.60 3.70 0 ‘ 1*1*11’ )’ m/ Z 82.00 43.62% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 '' i ■11 ■ I'1111r 11111 ■ ■ ■ i ■ ■11111111 3.20 3.30 3.40 3.50 3.60 3.70 47 m/ z 40.10 34.30%

0 ' i ' 1 1 ■ i ' 1 1 r i ' I ' ' |l|ll 1 " 11 ‘IB ■ । • ■ ■ ■ । । । । 1 > ‘ । m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 714

3.20 3.30 3.40 3.50 3.60 3.70 5000 82 m/ z 76.00 33.98% 47 35 12 261 0! ■ 1 I 1 ■ 1 I I ' 1,1 I 1 1 1 । । । । । ......................... ' m-1 , 108 1 1 i ■ ' 1 1 i ' 1 1 1 1 1 1 IFI n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115343: Thiirane, methyl- > > । ■ ■ ■ ■ 1 '' 11'111 ■ '1' 11111 111111 41 74 3.20 3.30 3.40 3.50 3.60 3.70 m/ Z 35.10 28.38%

5000

47 27 33 , 0 -----4 11,,,53.59..68, 'I ' i 1 " ■ i " ■ । i ■ ■ " । । " 1 I 1' i11 ■ ■ I ‘ I‘‘‘‘1‘1+1++L‘‘I‘+‘‘I /z-> 10 20 30 40 50 60 70 80 90 100 110 3.20 3.30 3.40 3.50 3.60 3.70

07768 .D SCAN020403.M Fri Apr 05 14:32:42 2002 Page 4

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