GCMS analysis results for sample AE08324, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020419\08324.D Vial : 11 Acq On 19 Apr 2002 5:58 pm Operator: Nefliu Sample sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020418.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 3 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 3.64 0.31 ug/1 433217 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 78 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 74 3 3,3-Dichloropropyne 108 C3H2C12 1000222-23-9 28 4 Furan, 2-methyl-________________________ 82 C5H60 000534-22-5 7 Abundance Scan 95 (3.637 min): 08324.D (-89) (-) m/z 74.10 100.00% 74 82 5000 40 47 ------------ 3.20 3.40 3,60 3.80 4.00 , 55 ---l------- TIB 109 1 ' I ' 1 1 1 1 11 1 ''I 1 1 1 1 I m/z 82.00 59.73% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35

5000 82 Arm, 3.20 3.40 3.60 3.80 4.00 47 m/ z 76.00 34.61% ■ ■ । 1 ' ' 1 । 1 ■ ■ ' i ‘ ■ 1 ’ 1 I ' ' ' ' I ' mr1 > । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ । m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74 ............. ' ' I AA .............. 1 11 I 1 1 ' 1 I ■ ' 3.20 3.40 3.60 3.80 4.00 5000 82 m/ z 40.10 32.94% 47 35

m/z-> 12 ■ 1 i 1 1 1 1 i ■ 10 20 26,30. br40.. III50... ,6062.........70 । ■ [ 1 ■ ■ ’ । ■ 1il 80 . 108 -mni > । । । । । । i-| । । । । । 90 100 110 Abundance #28312: 3,3-Dichloropropyne 74 3.20 3.40 3.60 3.80 4.00 m/z 84.00 24.60%

5000 38 47 1 I 53 60 sno. m/z-> ' 1 i ' 1 1 1 i ' 10 20 28,30. |,40.., 1 I 1 । i-< | ■ ■ • > | । 50 60 70 < । 80 82 108 * 1 1 I > > । 1 I 1 1 1 > I 1 1 1 1 I 90 100 110 3.20 3.40 3.60 3.80 4.00

08324.D SCAN020418.M Fri May 03 09:04:35 2002 Page 5

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