GC/MS analysis results, sample AE09768, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\020507\09768.D Vial: 15 Acq On 8 May 2002 1:56 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C: \MSDCHEM\1\METHODS\SCAN020507 . M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 2 Acetonitrile, dichloro- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 3.65 0.65 ug/1 50369 1,4-Dichlorobenzene-d4 11.38

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 91 2 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 64 3 Allyl mercaptan 74 C3H6S 000870-23-5 25 4 Thiirane, methyl- 74 C3H6S 001072-43-1 9 Abundance Scan 97 (3.649 min). 09768. D (-90) (-) m/z 74.10 100.00% 74

82 5000 47 ' 11 ' ' —P MAt t । । । i-1 35 3.40 3.60 3.80 4.00 ................ .. 11455 ............... ■ i ■ ■ ■ ■ i ■ I . .1 109 'I1' 1 1 1 1-1I 1 1 1 ''I 1 1 ' 1 I m/ z 82.00 56.23% mfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #28338: Acetonitrile, dichloro- 74

5000 47 82 21—A 3.40 3.60 3.80 4.00 35 m/z 84.00 33.19% 1 ' I............. 26,1.11 I—. 2111 „MMAlas.s 12 . 108 l ■ i > ■ ■ 1 । < • ■ । I > ■ ■ ■ । ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #115342: Acetonitrile, dichloro- 74 35 ■ ■ > ■ । ■ ■ ■ ■ । ■ 1 । r1 1 1 1 i ' 1 1 3.40 3.60 3.80 4.00 5000 82 m/z 47.00 31.74% 47

■ ■ i ■ ■ ■ ■ । ■ 1 ■ । ■ I ' 1 ‘li 1 1 1 T-|-r-r-r->-|-r T31 1 1 । 1 1 1 1 i 1 1 1 1 i 1 1 1 1 i m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 MwhyWAMMWwwwt #28161: Allyl mercaptan 4n 74 3.40 3.60 3.80 4.00 m/ z 76.00 30.36% 5000

47

n/z-> - . 77-32 11 , , |l, 53 59 68,1 lri । । । । । । 1 । । 1 । । ! । 1 । । । , ' । 10 20 30 1

40। tri

50 | I I I I

60 | 1 I I I

70 | I

80 90 100 110 ________ A 3.60 AAM AA 1 1 I r ' 1 ' | ........ 1 | f 1 1 3.40 3.80 A ' i ' 11 4.00

09768.D SCAN020507.M Tue May 14 08:42:54 2002 Page 4

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