GC/MS analysis results, sample AE09768, May 2002

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Data File C:\MSDCHEM\1\DATA\020507\09768.D Vial: 15 Acq On 8 May 2002 1:56 am Operator: Nefliu Sample sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 2-Propanone, 1,1,1-trichloro- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 6.12 0.89 ug/1 69620 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual V1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 59 2 11- ecen-2-one 182 C12H220 005009-33-6 17 3 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 4 .be -d-Fructofuranose, 1,3,4-t... 288 C12H1608 1000151-08-8 9 Abundance ‘ Scan 518 (6.123 min): 09768.D (-512) (-) m/ z 43.05 100.00% 43

5000

1 ‘ ' I ' ′ । । ' ! . . । । । .171 । । । । 63 1 173 1 1 1'1‛llm 1101 ' * 125 83 1 1 11971, ' ' m 5.80 6.00 6.20 6.40 —TTTT 1 " rli 1 1 11111 > 11 > 11 r> 111 I I 1 | I I I 1111111 m/z 47.00 8.62% /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #3877: 2-Propanone, 1,1,1 -trichloro- 43

WAMMY-A"yo wWWo 5000 111 II ‘ 5.80 6.00 6.20 6.40 m/z 125.00 8.62% 15

n/z-> 4 27 +++++53 1 63 73 83 ' ' I’’ 97 110 125 ' I ' ' 1 ' I 111 ' I ■ ' ' ' I ' ' ' ' | ' ' ' I ' " ' | । । । J 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 | . I' । | । । | | । |

Abundance #5798:11 -Dodecen-2-one 43 58 ............. AAk ■ 1 1 I ■ ' ■ ■ I ■ 1 ■ 'I 1 I . ’ I I I I I I 5.80 6.00 6.20 6.40 5000 m/z 97.00 8.17% 71

82

m/z-> I " " I " " I " " 11 „1.96111144135149164182 T'11' i ‘1117 1'1 ‘ r11'111 ’1111" 11111' l1 '^f" 1111111111.11 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #7671: N-Acetylpyrrolidone ......................... ‘A ., 43 5.80 6.00 6.20 6.40 m/z 82.90 6.92% 5000 __

99 127 28 15 56 — 86 AAl n/z—> + HH 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 112 ■ i' ■" ।■11" " ।'1" ।। "11" " ।। 5.80 6.00 (6.20 6.40

09768.D SCAN020507.M Tue May 14 08:42:57 2002 Page 5

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