GCMS scan comments for sample AE11480, May 29, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11480.D Vial: 14 Acq On : 21 May 2002 9 :12 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 3 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.13 0.77 ug/1 55598 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 56 2 1 - Fluorononane 146 C9H19F 000463-18-3 9 3 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 4 Ethanol, 2-chloro-, acetate 122 C4H7C1O2 000542-58-5 9 Abundance 1 Scan 519 (6.128 min): 11480.D (-512) (-) m/ z 43.10 100.00% 43

5000

■ ' i ' ■ ' ' I 1 1 1 1 I ' ttCI . । । । । 84 97 125 5.80 6.00 6.20 6.40 n/z-> Of 10 —.—201113038.40 Illpi5051 11 60rl’63t’ni -72-----4117 70 80 90 100 110 120 130 140 150 m/z 125.00 11.24% Abundance #3877:2-Propanone, 1,1,1-trichloro- 43

------- 5000 5.80 6.00 6.20 6.40 m/z 97.00 8.46% 15

m/z-> 01 10 mL 27 36 TTt 20 30 40 50 50 63 76 83 97 110117 125 11 ■111111'11 ■1' ''i ■111 r" '‘‘’i1 "lri > ■ ■ > j ■ ■»> । 60 70 80 90 100 110 120 130 140 150 ■

Abundance #4248:1-Fluorononane 43

55 -5.80 6.00 A 6.20 6.40 5000 29 m/z 83.90 7.92% 70 84 97

o! ' ■ i ■ 15 ■1 ■ i ■ -436+4 +4 62 , „Z7llThT 1104111118 126 Ppi ri’l 146 '111>।i. ।... 1।।, ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #3861:2-Propanone, 1,1-dichloro- 1 . .............. ।।। 43 5.80 6.00 6.20 6.40 m/z 47.05 7.21%

5000

1 36 15 27 — 50 63 76 83 93 125 0 TTTTT 'I ■ ■1111 ' ■ ■ i ■ ■111 ‘■11■■ > <।■■•>।■■••।.■ • ■ ।. 1111 ■ < । j 11 n/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 5.80 6.00 6.20 6.40

11480.D SCAN020521.M Fri May 24 09:32:16 2002 Page 5

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