Laboratory report documenting GCMS analysis of sample AE11154 conducted on May 29, 2002.
NYC-WTC_000025542–000025555Folder label: “GCMS X 5/17/02 A 5/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\MSDCHEM\l\DATA\020521\11154.D Vial: 19 Acq On : 22 May 2002 2:08 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.12 0.60 ug/1 44835 1,4-Dichlorobenzene-d4 11.37 Hit# Of 5 Tentative ID MW MolForm CAS# Qual
“ 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 37 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 4 .bgta.-d-Fructofuranose , 1,3,4-t... 288 C12H1608 1000151-08-8 9 Abundance Scan 518 (6.123 min): 11154.D (-512) (-) m/z 43.10 100.00% 43
5000
■ ' ' । ■ ■ • ■ । ■ i 1 1 1 'i ' 117 r 37 49 63 82 88 97 117 125 5.80 6.00 6.20 6.40 01 IIIITIuuu/pu 1111111 111,1 11,1 pI1 ponniy I'l'i 1111 1) । ■ pep l, er m/z 125.00 9.58% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #3877:2-Propanone, 1,1,1 -trichloro- 43
5000 i ' ■ ■ ■ i 1 ' ■ ' i 5.80 6.00 6.20 6.40 m/z 82.00 8.06% 15
n/z-> 0- 10 L —++ 30 27 36 +49,55, 53 76 83 91 97 20 50 40 70 90 60 110117 125 ■ 1 1 ' 1 1 1 11,1 i ‘ ■1 ''i ""i" 11 । ■ ■ ■ 11 ■ ■ 80 100 110 120 130 Abundance #7671: N-Acetylpyrrolidone 43 AAA,A.. 5.80 6.00 6.20 6.40 5000 m/ z 47.00 6.94% 99 127 28 56 15 69 n/z- > 0- TII , . ..... Abundance 10 20 30 —- 1111/1111112..... 40 50 60 70 80 90 100 110 120 130 #109152:2-Propanone, 1,1-dichloro- MWpAMWl wjh ' ' I ' ' ' ' I ' ' ' ' I ■ ' 1 ‘I 43 5.80 6.00 6.20 6.40 m/z 96.90 6.58% 5000
27 — , 49 55 63 I 36 76 83 91 0 " i 1 " ITilM) ■ .iiii 1 , rl ' ' ■ ' l ■ 'l 1 ' 1 1 I ' ''■ 1 ! ■ > " । । 111 • 1 > 126 । 1 ■ ■ 1 | 1 ' .... I.... ' 1 i ' ‘ ' ■ 1 1 1 ' 1 1 1 1 1 1 । 1 । 1 • । n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.80 6.00 6.20 6.40
11154.D SCAN020521.M Fri May 24 09:23:29 2002 Page 4
NYC-WTC_000025549
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NYC-WTC_000025520
Laboratory report of GCMS analysis for sample AE10812 conducted on May 29, 2002, showing surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024652
GCMS analysis for sample AE11157 identifying other unknown compounds with a 2,4-DDD surrogate recovery of 91%, completed May 22, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000022526
Laboratory report of GCMS analysis for sample AE11425 conducted on May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024851
GCMS analysis results for sample AE10245 conducted May 28, 2002, showing unknown compounds and 2,4-DDD surrogate recovery at 86 percent.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000025568
GCMS analysis report for sample AE11567 showing unknown compounds and surrogate recovery data from May 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024896
Laboratory report of GCMS analysis for sample AE10247 conducted on May 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000024390
Chain of custody record for GCMS analysis of sample AE10240 on May 20, 2002, including surrogate compound data.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043806
Analytical report for sample AE09769 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000043779
Analytical report for sample AE09767 documenting GC/MS analysis of unknown compounds and surrogate recovery data from May 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046147
Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10132 on May 17, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045748
Gas chromatography-mass spectrometry analysis of sample AE10701 conducted May 20, 2002, detecting unknown compounds and 2,4-DDD at 82% recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000045778
Gas chromatography-mass spectrometry report for sample AE10703 showing detection of unknown compounds and surrogate recovery.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000025494
Department of Environmental Protection administrative record sheet for World Trade Center site activities dated May 2002.
Filed in the same folder
NYC-WTC_000025495
Laboratory log sheet recording Method 608 extraction parameters and sample counts for sample AE11423 in May 2002.
Filed in the same folder
NYC-WTC_000025499
Laboratory report showing non-detect levels for 15 volatile organic compounds in a GCMS method blank processed on May 17-21, 2002.
Filed in the same folder
NYC-WTC_000025508
Laboratory report of GCMS calibration data showing response values and detection limits for 15 volatile organic compounds on May 17-21, 2002.
Filed in the same folder
NYC-WTC_000025512
Laboratory report of GCMS reference standard analysis showing response values for 15 volatile organic compounds on May 17-21, 2002.
Filed in the same folder