GCMS sample analysis results for unknowns, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020513\10130.D Vial: 17 Acq On : 14 May 2002 4:23 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.13 0.53 ug/1 41889 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

- 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C130 000918-00-3 43 2 N-Acet/lpyrrolidone 127 C6H9NO2 000932-17-2 9 3 5-Acetoxytridecane 242 C15H3 0O2 1000245-61-5 9 4 1,3,5/-Tri-O-acetyl-2,4-di-O-meth. . . 320 C14H2408 081703-39-1 9 Abundance / Scan 519 (6.129 min): 10130.D (-513) (-) m/ z 43.10 100.00% 40

5000

11117 ** I ■ ■ i 1 1 1 1 i 5.80 6.00 6.20 6.40 TET , I, . 83 , 125.................. 281 .................................. 539 '7 r 1 11 I ' 1 1 r i r ' 1 1 1 1 1 ' 1 i 1 ' ( 1 i ' 1 ' ’ i ' r ' ' i ' 1 1 1 i 1 1 1 1 I 1 1 1 ' I m/z 46.95 8.67% n/z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #3877: 2-Propanone, 1,1,1 -trichloro- 43

5000 MArMMN 5.80 6.00 6.20 6.40 m/z 125.00 8.21% 15 Ja .1 a 83 L l, 125 : 11 I 1 1 ' 1 I T •I I 'I ' i 1 ' ' 1 i ' 1 1 1 i 1 ' ■ ■ i ■ ' ■ ■ i ' 1 ' 1 i ' ■ 1 1 I ' 1 1 ' i ' ■ ■ 1 I lz-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #7671: N-Acetylpyrrolidone 43 ................ .. .................... > < । i < i ' r> ' » r | 1 I I » TBttt | 5.80 6.00 6.20 6.40 5000 m/z 83.00 6.05% 99 127 69 1 4,4l.1 r ‘ I‘ ‘I‘‘‘*1++/1**[**| Tl/Z-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #4231:5-Acetoxytridecane Pp—A 43 5.80 6.00 6.20 6.40 m/ z !96.95 5.59%

5000

1 ,69 97 129

2777--1- 19 .. 1 A. 1.. ■ ■ । ■ i ■ ■ ■ . । । . .1 । । । । । । Tl/Z--> 50 100 150 200 250 300 350 400 450 500 5.80 6.00 6.20 6.40

10130.D SCAN020507.M Tue May 14 15:58:26 2002 Page 3

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