GCMS analysis results for sample AE10812, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020521\10812.D Vial: 18 Acq On : 22 May 2002 1:09 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 2-Propanone, 1,1,1-trichloro- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.12 0.51 ug/1 38367 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

*-- 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 25 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 Undecanal 170 C11H220 000112-44-7 9 4 1- (2 Chlorophenyl)propan-2-one 168 C9H9C1O 006305-95-9 9 Abundance Scan 518 (6.123 min): 10812.D (-512) (-) m/ z 43.10 100.00% 43

5000

125 5.80 6.00 6.20 6.40 0- 153 82101 ...... 221,_ 421 m/z 125.00 11.37% m/z-> 0 50 100 150 200 250 300 350 400 Abundance #3877:2-Propanone, 1,1,1-trichloro- 43

5000 -.......... 1,94....... 1 5.80 6.00 6.20 6.40 m/z 47.00 6.58% 15 83 0 1 * j h 63 125 fotnn", i । । । । । । i i । i । । । । , । r ~ i j । । । । > /z-> 0 50 100 150 200 250 . 300 350 400 Abundance #7671: N-Acetylpyrrolidone 43

5.80 6.00 6.20 6.40 5000 m/z 127.00 6.31% 99 127

miz-> 0- 0 1541469,1 , 50 100 150 200 250 300 350 400 Abundance #109568: Undecanal 43 5.80 6.00 6.20 6.40 m/z 82.00 5.81% 82 5000

I 126

/z-> 0- 0 50 407.1 152 ... 100 150 200 250 300 350 400 5.80 ill I. 6,00 6.20 6.40 "T

10812.D SCAN020521.M Fri May 24 09:21:53 2002 Page 4

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