GCMS analysis results for sample AE11155, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11155.D Vial: 21 Acq On : 16 May 2002 7:34 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 6 2-Propanone, 1,1,1-trichloro- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

6.12 0.92 ug/1 69124 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual

2 1 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 64 2 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 3 2-Propanone, 1,1-dichloro- 126 C3H4C120 000513-88-2 9 4 2- tanone, 4-chloro-4,4-difluoro- 142 C4H5C1F2O 001515-16-8 9 Abundanc Scan 517 (6.117 min): 11155.D (-510) (-) m/z 43.10 100.00% 43

5000

97 127 5.80 6.00 6.20 6.40 T m/z 127.00 7.82% /z—> 0 50 100 150 200 250 300 350 400 450 Abundance #3877: 2-Propanone, 1,1,1-trichloro- 43

5000 A— ■ । ■ i 5.80 6.00 6.20 6.40 m/ z 97.10 7.68% 15 83 125 -ydk—h, I | I I i r । ■" I I I | i i I I | i I ' ' ■ Tl/z-> 0 50 100 150 200 250 300 350 400 450 Abundance #7671: N-Acetylpyrrolidone 43 A. NAA ----- 5.80 6.00 6.20 6.40 5000 m/z 82.00 7.15%

99 127

Tl/Z-> 0 44I50162,1,100,. 150 1 200 250 300 350 400 450 Abundance 43 #109152:2-Propanone, 1,1-dichloro- —A Bi 5.80 6.00 6.20 6.40 m/z 125.00 7.05% 5000 A

j .83126........................................... A..........Hu.......... 1 ■11' ■ ■11 ■ ■ ■11' ■ > > । । । m/z—> 0 50 100 150 200 250 300 350 400 450 5.80 6.00 6.20 6.40

11155.D SCAN020507.M Thu May 16 09:35:00 2002 Page 8

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