GCMS sample analysis results for unknowns, May 2002

Machine-extracted title · confidence 95%

Laboratory report listing GCMS results for unknown compounds and surrogates from sample AE10133 on May 17, 2002.

NYC-WTC_000046180–000046191

Folder label: “GCMS X 5/7/02 A 5/14/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020513\10133 .D Vial: 20 Acq On : 14 May 2002 7:22 am Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 2-Propanone, 1,1,1-trichloro- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.12 0.54 ug/1 43676 1,4-Dichlorobenzene-d4 11.38

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, 1,1,1-trichloro- 160 C3H3C13O 000918-00-3 38 2 1H-zonine, octahydro- 127 C8H17N 005661-71-2 9 3 IH-Azonine, octahydro- 127 C8H17N 005661-71-2 9 4 N-Acetylpyrrolidone 127 C6H9NO2 000932-17-2 9 Abundan Scan 518 (6.123 min): 10133.D (-513) (-) m/z 43.05 100.00% 43

5000

1 । । 1 1 । । । 1 । ' ' I ' ' TTI I I I ! | 5.80 6.00 6.40 161 82 97 112125 I 1 I I 1 > fOTT’ 11 /1tiu I I I I I I 1I pnpenuim ' I I I I I I I I I I I I rTgui I I I I I I I I I I I I I 295 I I I 1 T m/z 125.00 6.20 11.59% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #3877: 2-Propanone, 1,1,1 -trichloro- 43

5000 ................ All....................... ' ■ r i ■ ■ ■ 1 i 1 ■ 1 1 I 1 1 1 1 I ' 1 1 ' I 5.80 6.00 6.20 6.40 m/z 42.00 7.65% 15 I 29 1 1*1 63 83 97 110 125...... hpi+ri ||’'11111 * T‘11'T 11 1 । | 1 । । 1 | m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #108185:1H-Azonine, octahydro- 33 56 —*pr*fr“f 70 5.80 6.00 6.20 6.40 5000 m/z 82.10 6.00% 127 84 98 15 , ! | I A +4 4 1 — I I I 1 1 4 I I I | I 4, I I I I | I - | I I I I | I I I I | I I I I | | '' 41 14 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #744: 1 H-Azonine, octahydro- ।।I। । ii1। i ।। U 11 r ■ i ■ ■ ■ ■ i 33 5.80 6.00 6.20 6.40 56 m/z 127.00 5.22% 70 5000 127 84 98

/z-> 15 1411 W 20 40 60 1 112 ---PPTT 80 100 120 140 160 180 200 220 240 260 280 300 r 11 ■ i I‘114 I —.... 01....... 5.80 6.00 6.20 6.40

10133.D SCAN020507.M Wed May 15 08:28:51 2002 Page 3

NYC-WTC_000046186

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GCMS analysis results, sample AE10135, May 2002 · Box DEP Box 25

NYC-WTC_000046192

Gas chromatography-mass spectrometry analysis of sample AE10135 performed May 17, 2002, detecting unknown compounds and 2,4-DDD surrogate at 96% recovery.

1 shared topics · Same agency, volume and box · similarity 0.997